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Question: How do you pack a restaurant on opening night? Answer: You have a big following. And that's exactly what happened this weekend when Bouche Bistro, Chef Charles Dale's new eatery, opened in Santa Fe. Dale took over the vintage adobe building on West Alameda Street that formerly housed Agua Santa.
Dale came to Santa Fe from Aspen in 2008 to open Terra, at the then-new, Auberge Encantado Resort (now the Four Seasons Resort Rancho Encantado). He left when the mega-chain took over last fall. Luckily, he opted to stay in town and open his petite bistro.
We stopped by a few weeks ago to chat with the chef about his new project. We didn't think he'd make his projected opening, February 22nd, but this seasoned restaurateur (he previously owned two popular Aspen dining spots) made it.
We were there for dinner on opening night. The cozy banquette seating brought back memories of dining at Les Halles in New York City In the pre-Anthony Bourdain days. Bouche feels more like New York or Paris than Santa Fe and on opening night, it was a very urbane crowd.
The menu is French Bistro with a bit of Santa Fe thrown in. The oblong menu sits at your place and will remain there for you to take home if you wish. There are small plates, Seasonal Salads, Entrees, Sides and Desserts listed. It was a cold night and Steve started with a bowl of their rich onion soup followed by the small size portion of mussels. The house-baked sourdough is a great tool for sopping up the wine-infused broth that has just the right amount of red chile in it. I had the velvety foie gras (preparation differs nightly) and duck confit which came plated with white beans and kale. We were full and skipped dessert, though there were some decadent choices including a chocolate soufflé with the word "Nutella" in its name.
Good luck to Chef Dale and his new bistro. Bon appétit!
Bouche Bistro is a 451 West Alameda Street, (505) 982-6297 (enter on Water Street). They are serving dinner Tuesday through Sunday from 5:30 to 9:30pm. Reservations are strongly recommended.
We did an interview with Chef Dale when he was at Terra. At the time, he generously shared his Lobster Mac 'n Cheese with Mushrooms recipe. Mac 'n Cheese is still in the menu and with this recipe, you can make it at home. At Bouche, it comes in a covered pot and you can order it "au natural, with wild mushrooms or a bit of foie gras.


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Pregled bibliografske jedinice broj: 454371
De novo differentiation of intestinal villous M cells in weaned pigs immunized with levamisole-adjuvanted vaccine candidate F4ac+ or F18ac+ non-enterotoxigenic Escherichia coli strains
De novo differentiation of intestinal villous M cells in weaned pigs immunized with levamisole-adjuvanted vaccine candidate F4ac+ or F18ac+ non-enterotoxigenic Escherichia coli strains // Veterinarska Arhiv, 81 (2011), 1; 77-90 (međunarodna recenzija, članak, znanstveni)
De novo differentiation of intestinal villous M cells in weaned pigs immunized with levamisole-adjuvanted vaccine candidate F4ac+ or F18ac+ non-enterotoxigenic Escherichia coli strains
Kovšca Janjatović, Ana ; Lacković, Gordana ; Božić, Frane ; Valpotić, Hrvoje ; Tominac-Trcin, Mirna ; Sladoljev, Srećko ; Šeol, Branka ; Valpotić, Ivica ; Popović, Maja
Veterinarska Arhiv (0372-5480) 81 (2011), 1; 77-90
Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni
Ključne riječi
M cells; levamisole adjuvanticity; E. coli vaccines; weaned pigs
(M stanice; adjuvantnost levamisola; E. coli vakcine; odbijena prasad)
Active immunization against porcine postweaning colidiarrhea (CD) and/or colienterotoxemia (CE) caused by F4+ and/or F18+ enterotoxigenic Escherichia coli (ETEC) is still an unsolved problem. The intestinal microfold (M) cells play role in entry/invasion of intraluminal pathogens (such as ETEC strains), in antigen sampling, and in facilitating induction of immunity to gut infections. Just as ETEC strains can exploit M cells as the portal of entry for infections such as CD and/or CE, their high transcytotic ability make them an attractive target for mucosally delivered vaccines, adjuvants and therapeutics. The objective of our study was to evaluate the effects of levamisole-adjuvanted vaccine candidate F4ac+ and F18ac+non-ETEC strains on incidence/fequency of ileal M cells and up-regulation of antigen delivery by de novo formation of these cells in weaned pigs. Conventionally reared 4-weeks-old pigs were divided into three groups of which two were parenterally and orally immunized with levamisole (at Days -2, -1 and 0) in combination with either vaccine candidate non-ETEC strain (at Day 0), respectively. The third group of pigs received saline as a placebo. Challenge was performed (at Day 7) with F4ac+ ETEC strain, and the pigs were euthanatized (at Day 13) and sampled for immunohistology. Distribution patterns of cytokeratin 18 positive M cells revealed that they are rather solitary interspersed between enterocytes than as small clusters, and most of them were found to be located at the apex of villi in the ileum of 6-weeks-old pigs. Morphometric quantification of M cells in the ileal mucosa showed that levamisole-pretreated F18ac+non-ETEC-immunized and challenged pigs had significantly increased numbers (p<0.01) of ileal M cells as compared to the values obtained in the control nonprimed and challenged pigs. The proportion of these cells in this group of pigs was increased for 145%. In the levamisole-pretreated F4ac+ non-ETEC-immunized and challenged pigs only slightly increased (for 7%) proportion of M cells was recorded. However, this increase was not significantly different from the numerical values obtained for control pigs. Our finding that levamisole-adjuvanted F18ac+non-ETEC vaccine may affect de novo differentiation of antigen-sampling M cells by increasing their number in the ileum, indicated that the vaccine probably utilizes these cells as a target for entry/delivery to the nerby lymphocytes and induces protective immunity against CE. On the other hand, the failure of levamisole-adjuvanted F4ac+non-ETEC vaccine to produce a similar effect on M cells remains to be elucidated.
Izvorni jezik
Znanstvena područja
Veterinarska medicina
Projekt / tema
053-0532265-2248 - Imunomodulacijsko djelovanje levamisola kod svinja (Frane Božić, )
053-0532265-2255 - Kolidiareja i kolienterotoksemija prasadi : mukozna imunost i imunomodulacija (Maja Popović, )
119-1193080-3171 - Razvojna i populacijska biologija velikih morskih kralježnjaka u Jadranskom moru (Gordana Lacković-Venturin, )
Veterinarski fakultet, Zagreb
Časopis indeksira:
- Web of Science Core Collection (WoSCC)
- Science Citation Index Expanded (SCI-EXP)
- SCI-EXP, SSCI i/ili A&HCI
- Scopus


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Bots, Bugs, And Babes - Episode #54: The Hideous Sun Demon (1959): "Liquor and science don't mix well, apparently."
Manage episode 229177269 series 1232991
"Don't cry, Ann...Perhaps you should cry. The rest of us've got to have any hope that this life was....not wasted."
On this episode of Bots, Bugs, and Babes; my father (Al Jaconetti) and I celebrate our 3 Year Anniversary as we look back at the 60th anniversary of The Hideous Sun Demon (1959). Dad and I will explore all the different aspects of this film, from production to special effects, to how many the film was put together in a way that is unique to this film. So grab your sun screen, fire up your convertable, and learn how the blaze of the sun made him a monster!
Feedback for this show can be sent to: email@example.com
69 episodes


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Definition of imbed
The word imbed uses 5 letters:bdeim.
IMBED is playable in:
v. t. - To sink or lay, as in a bed; to deposit in a partly inclosing mass, as of clay or mortar; to cover, as with earth, sand, etc. 2
Direct anagrams of imbed
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HMCS Cataraqui Hosts Exercise RIDEAU GUARD
The sailors of several divisions of the Naval Reserve in Ontario were aboard HMCS Cataraqui on October 18 and 19 to participate in exercise RIDEAU GUARD in Kingston Harbour.
This exercise provided the opportunity for reservists from the Royal Canadian Navy (RCN) to update and practice their skills regarding light craft exercises, emergency planning, communications and other tasks which Naval Reservists could be called upon to exercise in the name of the Government of Canada.
Sailors who participated in exercise RIDEAU GUARD demonstrated professionalism and dedication towards the RCN. Naval Reservists of the RCN are fully engaged in their civilian lives while pursuing a military career. In fact, they participated in the exercise over the weekend, while still fulfilling their professional and personal obligations during the week.
Press release, Image: Canadian Navy


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Home » Casting calls » Studio set up to shoot flour and powder !!!!!
Studio set up to shoot flour and powder !!!!!
Natural Light Spaces is looking to be paid by a photographer or a model for this casting. It's based around Weedon Bec, Northampton NN7, UK Added 1524675303.
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www.naturallightspaces.co.uk to book :)
Natural Light SpacesStudio
The studio has been open for more than 3 years.
I'm based in Weedon Bec, Northampton NN7, UK. Map
Other castings by Natural Light Spaces
|The amazing duo skills of Tillie Feather and Leon Lift...A work shop with Lighting by JTD
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Cultural Resources Review and Impact Evaluation: Plymouth Village Sewage Separation Program, Project No. 1371-04
Author(s): Howard R. Sargent
Year: 1980
This resource is a citation record only, the Center for Digital Antiquity does not have a copy of this document. The information in this record has been migrated into tDAR from the National Archaeological Database Reports Module (NADB-R) and updated. Most NADB-R records consist of a document citation and other metadata but do not have the documents themselves uploaded.
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Cite this Record
Cultural Resources Review and Impact Evaluation: Plymouth Village Sewage Separation Program, Project No. 1371-04. Howard R. Sargent. 1980 ( tDAR id: 157989)
This Resource is Part of the Following Collections
Site Type
Investigation Types
Archaeological Overview • Site Evaluation / Testing
Cultural Resource • Sewer Construction • Site Settlement • Statement For Management
Geographic Keywords
33009 (Fips Code) • Grafton (County) • New Hampshire (State / Territory) • North America (Continent) • Pemigewasset River • Plymouth • United States of America (Country)
Temporal Keywords
Spatial Coverage
min long: -72.335; min lat: 43.528 ; max long: -71.347; max lat: 44.407 ;
Individual & Institutional Roles
Sponsor(s): Environmental Engineers, Inc.
Prepared By(s): Howard R. Sargent
Record Identifiers
NADB document id number(s): 7719
NADB citation id number(s): 000000083571
General Note: Submitted to: Environmental Engineers, Inc.
General Note: Sent from: Howard R. Sargent
General Note: Contract number: 1371-04


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Australia, France, Italy: Speed Cameras Sliced - [image: Rammed speed camera]On Sunday, vigilantes in Plemet, France, toppled one of the next-generation turret speed cameras that officials installed on th...
46 minutes ago
Writer's Email: firstname.lastname@example.com
Fone WST... +1318.717.9017
"The more corrupt the state, the more numerous the laws." ~ Gaius Cornelius Tacitus
UPDATE: t a messina lsu controversy finally cleared up
t.a. messina is running for alexandria marshal. on his website he claims to have played football for lsu from 1977 to 1979:
i e-mailed michael bonnette, sports information director for lsu football and asked for the official roster for those years.
my e-mail was answered by brianne mickles, an assistant in that department. she sent a pdf file of the official rosters from 1978 and '79. she said '77 was unavailable when i made the request.
according to the official roster, there is no messina listed for the years in question.
i think that anyone who falsely claims to be one of our beloved fighting tigers should be horsewhipped and fed to mike.according to the sec'y of state's website there are four candidates vying for alexandria city marshal:
Posted by wst... at 09:16


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|2019-11-09 12:59
Proposal to end school lunch shaming moves ahead...
BANGOR, Maine (AP) - A federal proposal designed to prevent lunch shaming has moved ahead thanks to a vote in the U.S. Senate. Republican Sen. Susan Collins of Maine and Democratic Sen. Tom Udall of New Mexico added an amendment to a funding bill that wou...


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Clip the dog's nails.[3] If left untrimmed, a dog's nails can curl under into the paw pads or twist toes in a way that causes joint damage. To keep your dog's nails short, clip them regularly, depending on how fast his nails grow. If you can hear his nails on the ground when he walks, that means his nails are touching the ground, and are too long. [4]
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In addition, people with pet dogs took considerably more physical exercise than those with cats and those without pets. The results provide evidence that keeping pets may have positive effects on human health and behaviour, and that for guardians of dogs these effects are relatively long-term.[195] Pet guardianship has also been associated with increased coronary artery disease survival, with human guardians being significantly less likely to die within one year of an acute myocardial infarction than those who did not own dogs.[196]
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^ Jump up to: a b Thalmann, O.; Shapiro, B.; Cui, P.; Schuenemann, V.J.; Sawyer, S.K.; Greenfield, D.L.; Germonpre, M.B.; Sablin, M.V.; Lopez-Giraldez, F.; Domingo-Roura, X.; Napierala, H.; Uerpmann, H.-P.; Loponte, D.M.; Acosta, A.A.; Giemsch, L.; Schmitz, R.W.; Worthington, B.; Buikstra, J.E.; Druzhkova, A.; Graphodatsky, A.S.; Ovodov, N.D.; Wahlberg, N.; Freedman, A.H.; Schweizer, R.M.; Koepfli, K.- P.; Leonard, J.A.; Meyer, M.; Krause, J.; Paabo, S.; et al. (2013). "Complete Mitochondrial Genomes of Ancient Canids Suggest a European Origin of Domestic Dogs". Science. 342 (6160): 871–874. Bibcode:2013Sci...342..871T. doi:10.1126/science.1243650. hdl:10261/88173. PMID 24233726.
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We continually review and update our pet grooming policies, procedures and standards, under the supervision of our Director of Veterinary Medicine, with counsel from a number of independent experts in animal care, behavior and ethics. We continue to train our teams on and reinforce the critical importance of following those policies at all times. Since 2015, we've worked together with the Pet Industry Joint Advisory Council (PIJAC) and the Professional Pet Groomers & Stylists Alliance (PPGSA) to encourage and support national health and safety standards for the grooming industry. We believe these standards are critical to the wellbeing of pets everywhere, and we continue to work with other pet industry leaders to encourage industry-wide adoption and adherence to them.


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- Elecampane is used in traditional western herbal medicine (WHM) for the symptomatic relief of persistent mild bronchial cough
- Echinacea may help ease symptoms associated with mild upper respiratory tract infections (URTIs) and the common cold when taken at the first sign of infection.
- The formulation also includes thyme, ivy leaf, marshmallow, mullein and zinc
- The formula is naturally flavoured with honey and manuka honey with no artificial colours, flavours or sweeteners
No added dairy, gluten, shellfish, soy protein, yeast
Dosage & warnings
Adults and children over 13 years: 10 mL 3 times daily
Children 6 - 12 years: 5 mL 3 times daily
Children 3 - 5 years: 2½ mL 3 times daily
Contains potassium sorbate and honey
Not to be used in children under two years of age without medical advice
If coughing persists consult your healthcare professional
Vitamin and mineral supplements should not replace a balanced diet
Always read the label
Use only as directed
Only take as directed.
1 serve
|Echinacea angustifolia (root)
equiv. Alkylamides
equiv. Cichoric acid
|100 mg
0.92 μg
183.3 mg
|Inula helenium (root) ext. equiv. dry (Elecampane)
|150 mg
|Althaea officinalis (root) ext. equiv. dry (Marshmallow)
|300 mg
|Verbascum thapsus (leaf) ext. equiv. dry (Mullein)
|100 mg
|Thymus vulgaris (herb) ext. equiv. dry (Thyme)
|100 mg
|Zinc gluconate
equiv. Zinc
|3.8 mg
0.5 mg
|Hedera helix (leaf) (Ivy)
equiv. Hedreracoside C
|22.8 mg
456 μg


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A weird happening occurred the other day in Queensland, Australia, when a wild kangaroo was crossing the road and bumped into a cyclist, knocking him on the ground. It seems that the cyclist survived the accident but he suffered a knee injury.
Published on February 1, 2018 by VidReactor
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Skinner, James among athletes with Arizona ties taking aim at Rio
By Kendall Pope | Wednesday, April 27, 2016
MyKayla Skinner's siblings got her started in gymnastics.
Ted Cruz, GOP supporters rally in Phoenix ahead of Tuesday election
By Ben Margiott | Friday, March 18, 2016
More than 2,000 Ted Cruz supporters rallied for his cause Friday night in Phoenix, but his campaign event was just as much a rally for the GOP.
Black History Month: West Valley woman helping others return to college
By Brandi Henry | Wednesday, Feb. 24, 2016
Janet Denson, owner of Love Images, a nonprofit organization, makes scholarships and other resources available for women over 25 who want to return to college. [Read more Black History Month stories]
With two clutch plays, special teams spur Alabama to championship in Glendale
By Bill Slane | Tuesday, Jan. 12, 2016
It's a third of the game. It's a phrase every football fan has heard a thousand times over -- special teams is a third of the game.
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Theranos, a blood testing company and lab that operates in 40 different Walgreens around the Valley, has been scrutinized for its proprietary technology and methods. But that does not mean the Arizona law that allows patients to obtain blood tests and results without prior review by a doctor - a law that Theranos helped author - is in jeopardy.
One West Valley community's ever-shifting demographics reflect changing face of Phoenix
By Erica Lang | Wednesday, Dec. 16, 2015
Where the city of Phoenix once ended at 83rd Avenue, onion fields began — stretching into the distance in a nearly straight shot to Luke Air Force Base. Almost 50 years later, the ground that once supported agriculture now reflects a community whose roots prove ever changing.
Suns help ready 'Madhouse' for team's return to its former home
By Chris Caraveo | Friday, Sept. 25, 2015
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PHOENIX – Last night's main Republican presidential debate covered a wide range of issues including immigration and border enforcement. Cronkite News checked the facts behind some of the candidates' statements.
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Which digital piano is the best for music production?
Which piano is the best that has following features:
- 88 weighted keys
pure sound
- good quality
- connects to computer (compatible with FL Studio)
- not super expensive
4 Answers
- MamiankaLv 73 weeks agoFavorite Answer
Unless you are a trained pianist using this for serious practice/live performance - go with synth action, not weighted. Save $$, and I don't you need weighted. Most decent kybds have good sampled sound, or it is in the banks of good notation/production software.They all connect to your computer and software. I have been doing this since around 1975 - still.do. You have a lot of choices, so do some research for price and reputable makers.
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This thoughtful couple's prayer book is part of the Rob and Joanna Teigen collection. It is perfect for spouses looking to connect on a deeper, more spiritual level. 101 Prayers for Mr. & Mrs. will enable couples to daily commit their relationship to the Lord with the easy to follow Scriptures.
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text:
Electron irradiation process of glass passivated semiconductor devices for improved reverse characteristics
Semiconductor devices with improved reverse characteristics are obtained by exposing the semiconductor bodies of the devices that are passivated by alkali-free glasses to a high energy radiation such as an electron radiation so as to shorten a life time of the bodies down to a predetermined value, while increasing the reverse leakage current of the bodies, and by subjecting the irradiated semiconductor bodies to an annealing treatment at a temperature of 250.degree. to 350.degree. C. for a sufficient time so as to decrease the reverse leakage current down to a predetermined value, while maintaining the order of the shortened life time.
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The present invention relates to a process for manufacturing a semiconductor device having a glass coating on the surface of a p-n junction formed in a semiconductor body of the device, and more particularly to a process for manufacturing a semiconductor device with improved reverse characteristics.
It is well known in the art that in order to perform a high speed switching operation of semiconductor devices such as diodes, transistors, and thyristors, carrier life time of the devices must be made small and that the life time can be shortened by forming recombination centers in semiconductor bodies of the devices. The recombination centers are formed by doping heavy metal atoms such as gold in the bodies or by irradiating the semiconductor bodies with radiation rays or beams to cause lattice defects therein. Since the irradiation method as disclosed in U.S. Pat. Nos. 3,852,612; 3,888,701; 3,809,582, and 3,872,493 has a number of advantages over the doping method, there is a tendency to increase the use of the former method.
On the other hand, the demand for semiconductor devices having high blocking voltages and reliability is increasing, and to this end, the surface of a p-n junction exposed to the surface of a semiconductor body is often passivated by alkali-free glass as disclosed in U.S. Pat. Nos. 3,486,871; 3,551,171; 3,778,242; 3,650,778; 3,752,701; 3,505,571; and 3,674,520. According to experiments by the inventors, it has been revealed that when semiconductor devices passivated by the glass are irradiated by an electron beam, the reverse leakage current of the p-n junction with the glass layer increases remarkably, while there has been observed only a moderate increase in the leakage current when the surface is passivated by resins or varnishes. Because of the increase in the reverse leakage current, heat generation in the blocked state of the device makes it difficult to keep the blocked state and brings about such inconveniences as an increase in the power loss and malfunctions of the devices as well.SUMMARY OF THE INVENTION
Accordingly, it is an object of the present invention to provide a method of manufacturing semiconductor devices passivated with a glass layer, which have improved reverse characteristics.
The process for manufacturing a semiconductor device of the present invention is characterized in that a glass layer for passivating the surface of a p-n junction exposed on the surface of a semiconductor body is irradiated by a radiation source to shorten the life time down to a predetermined value and then the semiconductor body and the glass layer are subjected to annealing at a temperature of 250.degree. to 350.degree. C. for a period of time sufficient to reduce a reverse leakage current having increased in the irradiation step down to a value smaller than the increased leakage current, while maintaining the degree of the life time shortened in the irradiation step. Preferably, increased leakage current should be reduced by the annealing to the same order of the leakage current value as measured before the irradiation.
The present invention will now be described in detail taken in conjunction with the accompanying drawings in which:BRIEF DESCRIPTION OF THE DRAWINGS
FIG. 1 is a sectional view of a silicon diode passivated with a glass layer in the step of irradiation with radiant rays.
FIG. 2 is a graph showing the relationship between annealing temperature and leakage current.
FIG. 3 is a graph showing the relationship between the annealing temperature and the reverse recovery time.
FIG. 4 is a graph showing the relationship between annealing time and carrier life time and reverse leakage current.
FIG. 5 is a graph showing the relationship between annealing time and annealing temperature.DETAILED DESCRIPTION OF PREFERRED EMBODIMENTS
Radiation rays or beams include electron beams, proton beams, neutron beams .alpha.-rays, .gamma.-rays, .beta.-rays, etc. as disclosed in the U.S. Pat. Nos. 3,852,612; 3,888,701; 3,809,582; and 3,872,493. Of these radiation beams and rays, preferable are electron beams from the practical point of view.
As the conditions for the irradiation are substantially the same as those employed in the conventional process such as disclosed in U.S. Pat. No. 3,872,493, detailed description of the conditions will be omitted to avoid superfluousness.
When an electron beam is employed, the minimum value of energy thereof which is necessary for causing lattice defects of the simple Frenkel type within the semiconductor body (Si) is about 0.5 MeV, and the minimum energy in case where the semiconductor body is irradiated indirectly with the electron beam through a glass layer, an electrode layer, a casing for the body, etc. is about 1 to 3 MeV or above.
The minimum dose of irradiation varies in dependence on a desired life time value, and it is generally above the order of 10.sup.13 electrons/cm.sup.2. Preferably, desired lifetime value is less than 50% of the value measured before the irradiation. If the value of exposure exceeds the order of 10.sup.16 electrons/cm.sup.2, the semiconductor body is too much irradiated, whereby a voltage drop in the conductive state of the device becomes very large such as 5 volts. Such a large voltage drop is not tolerable to practical use. Accordingly, the practical range of exposure is on the order of 10.sup.13 to 10.sup.16 electrons/cm.sup.2.
Semiconductor devices to be subjected to the irradiation are prepared by the conventional methods including the doping and passivation steps. In the present invention, the passivation is performed with a glass which is free of alkali atom ions and has a coefficient of linear thermal expansion approximate to that of the semiconductor body employed. A variety of glass compositions for use in passivation of semiconductor bodies have been proposed and are disclosed in U.S. Pat. Nos. 3,486,871; 3,551,171; 3,778,242; 3,650,778; 3,752,701 and 3,674,520. Typical glass compositions useful as a passivating glass layer for the devices of the present invention are (1) a ZnO--B.sub.2 O.sub.3 --SiO.sub.2 system, (2) a B.sub.2 O.sub.3 --PbO--SiO.sub.2 system, and (3) a ZnO--B.sub.2 O.sub.3 --SiO.sub.2 --PbO system. The glass compositions are selected to have a coefficient of linear thermal expansion of about 100.times.10.sup.-7 /.degree.C. or less, preferably 80.times.10.sup.-7 /.degree.C. or less over a temperature range of 100.degree. to 350.degree. C. Of the conventional alkali-free glasses, preferable compositions are shown as follows:
______________________________________ (1) ZnO 63% by weight B.sub.2 O.sub.3 20 by weight SiO.sub.2 9.4 by weight PbO 4.3 by weight Sb.sub.2 O.sub.3 0.5 by weight SnO.sub.2 1.2 by weight Al.sub.2 O.sub.3 0.09 by weight (2) ZnO 62% by weight B.sub.2 O.sub.3 20 by weight SiO.sub.2 9.5 by weight SnO.sub.2 0.7 by weight PbO 2.8 by weight Sb.sub.2 O.sub.3 1.5 by weight A1.sub.2 O.sub.3 0.1 by weight (3) ZnO 54% by weight B.sub.2 O.sub.3 16 by weight SiO.sub.2 7.8 by weight SnO.sub.2 1.1 by weight PbO 4.3 by weight Sb.sub.2 O.sub.3 0.4 by weight PbTiO.sub.3 12.3 by weight ______________________________________
Preferable glasses may be chosen within the following composition:
______________________________________ ZnO 50 to 80% by weight B.sub.2 O.sub.3 5 to 30% by weight SiO.sub.2 1 to 10% by weight PbO up to 10% by weight Sb.sub.2 O.sub.3 up to 5% by weight SnO.sub.2 up to 5% by weight Al.sub.2 O.sub.3 up to 5% by weight ______________________________________
Description will be made of annealing conditions suitable for glass passivated semiconductor devices having been subjected to such irradiation. In general, crystal defects caused in a semiconductor body by the irradiation with radiant rays or beams may be recovered by a heat treatment, i.e., annealing. Accordingly, when the semiconductor device subjected to the irradiation by the electron radiation is heat-treated at a high temperature, the recombination centers caused by the irradiation will be annihilated, so that the lift time of the device will become long. According to experiments by the inventors, however, it has been found that the reverse leakage current of a glass-passivated semiconductor device at the p-n junction as increased by the irradiation with the electron radiation can be made small when the device is annealed at a temperature of 250.degree. C. for 0.5 hour and may return to a small current value observed before the irradiation, while an undesirable increase in the life time takes place. The relation between the heat-treatment temperature and time which bring forth the same annealing effect is inversely proportional, and by way of example, a heat treatment of 300.degree. C. for 2 hours is equivalent to a heat treatment of 350.degree. C. for about 0.5 hour. Accordingly, preferable heat-treatment conditions are lower than equivalence to 350.degree. C. for 0.5 hour, but higher than equivalence to 350.degree. C. for 0.1 hour, and higher than equivalence to 250.degree. C. for 0.5 hour, but lower than equivalence to 250.degree. C. for 50 hours. A more desirable heat treatment is performed under conditions above equivalence to 250.degree. C. for 0.5 to 20 hours at which leakage current is substantially reduced, and below equivalence to 350.degree. C. for 0.5 to 0.1 hours. Accordingly, the annealing is carried out under the conditions defined by the temperature range and time range, i.e. 250.degree. C. for 0.5 to 50 hours to 350.degree. C. for 0.1 to 0.5 hour.
FIG. 1 is a drawing which shows a section of a glass mold type diode according to an embodiment of this invention. The diode 10 consists of a silicon pellet 1, an anode lead 2, a cathode lead 3, and a glass insulator 4 for passivating and protecting the silicon pellet 1. The silicon pellet 1 consists of a p.sup.+ diffused layer 11, an n-type high resistivity layer 12, an n.sup.+ diffused layer 13, and metal contacts 14, 15 of p.sup.+ and n.sup.+ layers. A p-n junction J is formed between the p.sup.+ diffused layer 11 and the n-type high resistivity layer 12. Such device is fabricated in the way stated below. Boron and phosphorus are successively diffused into both the principal surfaces of an n-type silicon wafer having a resistivity of 30.OMEGA.. cm and a thickness of about 270 .mu.m to respective amounts of about 70 .mu.m, to form the p.sup.+ and n.sup.+ layers 11 and 13. Subsequently, aluminum (Al) is evaporated as the metal contacts 14, 15, whereupon the wafer is cut into pellets each with a diameter of 1.4 mm, and the anode lead 2 and the cathode lead 3 are respectively bonded to the opposite principal surfaces of the pellet 1. Further, the globular glass insulator 4 is formed around the pellet 1 as shown in FIG. 1. In the glass coating treatment, zinc borosilicate series glass of the following composition was employed:
TABLE ______________________________________ Ingredient Ratios Ingredients (% by weight) ______________________________________ ZnO 63.1 B.sub.2 O.sub.3 20.47 SiO.sub.2 9.388 PbO 4.29 Sb.sub.2 O.sub.3 0.476 SnO.sub.2 1.23 Al.sub.2 O.sub.3 0.087 ______________________________________
The glass material is powdered and dispersed into water to form a slurry and is deposited on the periphery of the pellet 1 and end parts of the leads 2, 3 as shown in the figure. Thereafter, the deposited glass slurry was baked to fuse, whereby the surface of the p-n junction of the device 10 is passivated, and at the same time, the pellet is protected against a mechanical damage.
Subsequently, the device 10 is irradiated with electron radiation 16. In order to attain a uniform irradiation effect within the pellet 1, the energy of the election radiation was required to be about 2 MeV. Before the irradiation with the electron radiation, the leakage current of the device 10 was about 7.times.10.sup.-9 A (reverse bias: 400 V), the "on" voltage was about 1.0 V (forward current: 4 A), the recovery time in the reverse direction was about 7 .mu.s, the life time of carriers was about 8 .mu.s, and the blocking voltage was about 900 V, respectively. When the device 10 was subjected to the irradiation with electron radiation of an energy of 2 MeV and of the level of the irradiation dosage of 4.times.10.sup.13 to 5.times.10.sup.14 electrons/cm.sup.2, the life time of carriers and the recovery time in the reverse direction were shortened as expected, but the leakage current increased as unexpectedly as 100 times at the maximum. FIGS. 2 and 3 show the results of an isochronal annealing of 0.5 hr as to the samples. As is apparent from both the figures, the recovery time in the reverse direction is shortened to 1/3-1/15 of the value prior to the irradiation in accordance with the dosage level after the electron irradiation. Although the effect of irradiation may be eliminated by a heat treatment above 450.degree. C. for 0.5 hour, the shortened life times cannot be maintained unless the annealing is carried out at 350.degree. C. or below. Although not shown in the drawing, it has been confirmed that the life time of carriers exhibits quite the same tendency as that of the recovery time in the reverse direction. On the other hand, the leakage current begins to recover by a heat treatment above 200.degree. C., but such a relatively low temperature annealing requires a very long time to obtain desired results. Therefore, an annealing of 250.degree. C. for 0.5 hour is preferably chosen in case of, for example, the irradiation of 4.times.10.sup.13 electrons/cm.sup.2. In a case where an electron dosage of irradiation is large, annealing conditions under which the leakage current begins to decrease again are substantially the same. However, in case of the irradiation dosage of 5.times.10.sup.14 electrons/cm.sup.2, the leakage current is decreased by the heat treatment of 350.degree. C. for 0.5 hour without increasing the shortened lift time of the device. According to the combination of the irradiation and annealing, there is obtained the diode device 10 which has a shortened life time of carriers as determined by the conditions of the irradiation and a short recovery time characteristic and which has a small leakage current recovered to the same level as that measured before the irradiation.
FIG. 4 shows results at the time when the device 10 of FIG. 1 was subjected to the irradiation with electron radiation of an energy of 2 MeV and an electron dosage of 4.times.10.sup.14 electrons/cm.sup.2 and then to annealing at 300.degree. C. In the figure, a curve a represents the life time, and a curve b the leakage current in the reverse direction. While the life time begins to increase again after the annealing for above 5 hours at last, the leakage current begins to become small only after the annealing for 0.1 hour and becomes a value measured before the irradiation when the annealing is carried out for 2 hours. FIG. 5 is a graph which shows the relationship between the annealing time and the annealing temperature. A curve a, which corresponds to an irradiation dosage of a range from 1.times.10.sup.13 to 1.times.10.sup.16 electrons/cm.sup.2, represents the upper limit for the annealing conditions above which undesirable annealing effects begin to appear in the life time and the reverse recovery time irrespective of the irradiation dosage, while curves b.sub.1 and b.sub.2 represent the lower limit for the annealing conditions which are necessary to reduce the leakage current to the value measured before the irradiation. Curve b.sub.1 and curve b.sub.2 correspond to an irradiation dosage of 5.times.10.sup.14 electrons/cm.sup.2 and to an irradiation dosage of 4.times.10.sup.13 electrons/cm.sup.2, respectively. Annealing conditions lying between the curve a and the curve b.sub.1 or curve b.sub.2 are the conditions under which, while holding the life time etc. at values measured immediately after the electron irradiation, the inconvenient increase of the leakage current attributed to the irradiation can be reduced. In a case where the dosage of irradiation is as large as, for example, 1.times.10.sup.16 electrons/cm.sup.2, curves b.sub.1 and b.sub.2 will agree with or go beyond the curve a, but even in that case, the leakage current is reduced by annealing to a level close to that before the irradiation under conditions below the curve a. Although, in the embodiment, only the glass-molded element has been mentioned, the effect has been confirmed as to a device with a glass layer formed only in the vicinity of the exposed surface of a p-n junction, and the scope of application of this invention is not restricted to the present embodiment.
As is apparent from the above detailed description, while the life time of carriers and the turn "off" characteristics such as the reverse recovery time of a diode thereby governed are maintained at desired values determined by the conditions of irradiation, the disadvantage of the irradiation can be removed. That is, the increased leakage current of a glass passivated semiconductor device can be reduced. Since the life time is not affected during the annealing of the specified conditions, the control of the life time is very easy with the features of the irradiation.
While the novel principles of the invention have been described, it will be understood that various omissions, modifications and changes in these principles may be made by one skilled in the art without departing from the spirit and scope of the invention.
1. A process for manufacturing a semiconductor device having improved reverse characteristics comprising the steps of:
- (a) preparing a semiconductor assembly comprising a semiconductor body which has at least one p-n junction therein and first and second main surfaces at the both ends thereof, an edge face of the p-n junction being exposed to the body, and first and second electrodes each being in ohmic contact with the corresponding main surfaces,
- (b) forming a passivating coating of an alkali-free glass layer on the edge face to protect the body from mechanical damage thereto,
- (c) irradiating the semiconductor body through the coating to radiation rays sufficient to cause lattice defects in the body so as to shorten the life time of the minority carriers down to a predetermined value and to increase the reverse leak current at the p-n junction, and
- (d) annealing the semiconductor assembly after the irradiation, said annealing being carried out at an elevated temperature for a period of time sufficient to recover the electric characteristics damaged in the step of the irradiation, the annealing being carried out under such a condition that the increased reverse leak current is decreased to a predetermined value smaller than the increased value, while the degree of the shortened life time is substantially maintained during the annealing.
2. The process as defined in claim 1, wherein the glass layer has a coefficient of linear thermal expansion approximate to that of the semiconductor body.
3. The process as defined in claim 1, wherein the glass layer has the following composition:
4. The process as defined in claim 1, wherein the annealing is carried out under the condition corresponding to a condition not less than 0.5 hour at 250.degree. C. but not more than 0.5 hour at 350.degree. C.
5. The process as defined in claim 1, wherein the exposure to radiation is an amount corresponding to 1.times.10.sup.13 to 1.times.10.sup.16 electrons/cm.sup.2.
6. The process as defined in claim 1, wherein the annealing is carried out under the conditions defined by 250.degree. C. for 0.5 to 50 hours to 350.degree. C. for 0.1 to 0.5 hour.
7. A semiconductor device with shortened life time characteristics and improved reverse characteristics which comprises (1) a semiconductor body having at least one p-n junction therein exposed to a side face of the body and first and second main surfaces thereof at the opposite ends, (2) first and second electrodes being in ohmic contact with the first and second main surfaces, and (3) a glass coating for mechanically protecting the semiconductor body as well as passivating the edge face, wherein the glass coating in intimate contact with the edge face contains zinc oxide and boron oxide as main components but contain no atoms of alkali metals, the semiconductor body and the glass coating being subjected to irradiation through the coating to radiation rays sufficient to cause lattice defects in the body so as to shorten the life time of the minority carriers down to a predetermined value, and annealing at an elevated temperature for a period of time sufficient to recover the electric characteristics damaged in the step of the irradiation, the improvement that comprises employing as the coating an alkali-free glass layer, whereby a reverse leak current at the p-n junction is increased in the irradiation step, and the annealing is carried out under such condition so that the increased reverse leak current is decreased to a predetermined value smaller than the increased value, while the degree of the shortened life time is substantially maintained in the step of the annealing, whereby the reverse leak current is substantially reduced to a value smaller than that measured after the irradiation.
8. The semiconductor device as defined in claim 7, wherein the glass coating has the following composition:
9. The semiconductor device as defined in claim 7, wherein the glass coating has a linear thermal expansion of not more than 100.times.10.sup.-7 /.degree.C.
|April 1970
|July 1972
|Suzuki et al.
|August 1973
|September 1974
|Sakamoto et al.
|May 1975
|Cresswell et al.
|January 20, 1976
|Tarneja et al.
|December 7, 1976
|Goldberg et al.
|April 1976
Type: Grant
Filed: Aug 1, 1977
Date of Patent: May 6, 1980
Assignee: Hitachi, Ltd.
Inventors: Tomoyuki Tanaka (Hitachi), Toshikatsu Shirasawa (Hitachi), Masahiro Okamura (Hitachi)
Primary Examiner: L. Dewayne Rutledge
Assistant Examiner: Upendra Roy
Law Firm: Craig and Antonelli
Application Number: 5/820,698
International Classification: H01L 754; H01L 21263;


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110 - 4460 Chatterton Way
Victoria, BC
Canada V8X 5J2
(click to close)
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|December 2019
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I believe that it is my job to educate my clients and to help them make informed decisions. I never use high-pressure tactics and always leave the final decision up to you. After all, you are the one who has to be satisfied with the results in the end.
I have spent most of my adult life involved in some type of sales or marketing. Over the years I have become a highly skilled negotiator.
I believe in living life by the Golden Rule; "Do unto others as you would have them do unto you."
A portion of every sale is donated to my favourite charities. Both the Royal LePage Shelter Foundation and The Inside Ride do important and great work.
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