text:
|Publication number
|Publication type
|Application number
|Publication date
|Jun 27, 1989
|Filing date
|May 18, 1987
|Priority date
|May 18, 1987
|Fee status
|Publication number
|Hoang D. Vu
|Original Assignee
|The Procter & Gamble Company
|Export Citation
|BiBTeX, EndNote, RefMan
|Patent Citations (8), Referenced by (40), Classifications (17), Legal Events (5)
|External Links: USPTO, USPTO Assignment, Espacenet
The present invention relates to shampoo compositions which have improved hair conditioning and style retention properties due to the inclusion of particular types of silicone polymers which are premixed with a surfactant prior to addition to the total composition.
The desire to have hair retain a particular shape is widely held. The two methodologies of accomplishing this are permanent chemical alteration of the hair or a temporary alteration. A temporary alteration is one which can be removed by water or by shampooing. This has generally been accomplished by means of the application of a separate composition to dampened hair, i.e., after shampooing and/or conditioning, and prior to drying and/or styling. The materials used to provide setting benefits have generally been resins or gums and have been applied in the form of mousses, gels, lotions, and sprays. However, some people desire a high level of style retention in a single composition such as that provided by a separate composition without the negative impact of these materials on dry hair properties, particularly ease of combing and hair feel. Silicones can provide such benefits.
Silicones in various hair care compositions have been disclosed in a large number of different publications, including U.S. Pat. Nos. 3,964,500, to Drakoff, issued June 22, 1976; 4,364,837, to Pader, issued Dec. 21, 1981; 4,341,799, to Good, issued July 27, 1982; 4,465,619, to Boskamp, issued Aug. 14, 1984; 4,515,784, to Bogartus, issued May 7, 1985; 4,387,090, to Bolich, issued June 7, 1983; 4,529,586, to DeMarco et al, issued July 16, 1985; and 4,559,227, to Chardia et al, issued Dec. 17, 1985.
It has now been discovered that shampoo compositions comprising certain rigid silicone polymers and volatile carriers provide increased style retention and hair condition. The compositions provide the increased style retention to the hair without decreasing dry hair properties such as ease of combing. This improved performance is obtained by mixing the rigid silicone with a surfactant prior to mixing with the other shampoo components.
It is, therefore, an object of the present invention to provide shampoo compositions which contain a high molecular weight rigid silicone polymer dispersed in a surfactant paste premix prior to mixing with other shampoo components.
It is a further object of the present invention to provide stable shampoo compositions containing a volatile carrier.
It is a further object of the present invention to provide shampoo compositions providing good style retention.
It is a further object of the present invention to provide an improved method of temporarily styling and conditioning hair.
It is a further object of the present invention to provide a method of treating hair for improved style retention.
These and other objects will become readily apparent from the detailed description which follows.
Unless otherwise indicated, all percentages and ratios herein are by weight.
The present invention relates to hair care compositions comprising from about 0.01% to about 10% of a rigid silicone polymer, from about 0.1% to about 10% of a volatile carrier, from about 10% to about 35% of a synthetic surfactant, from about 0.2% to about 12% of about a 50% aqueous solution of alkyl glyceryl sulfonate, and water, wherein the rigid silicone is mixed with the sulfonate solution prior to mixing with the other shampoo component.
The essential as well as optional components are described below.
The compositions of the present invention contain at least one rigid silicone polymer which when applied to hair imparts style retention benefits.
The polymers comprise from about 0.01% to about 10% of the composition, preferably from about 0.05% to about 7%.
Polymers useful in the present invention include, but are not limited to, filler reinforced polydimethyl siloxane gums including those having end groups such as hydroxyl and resin reinforced siloxanes.
The rigid silicone polymers useful in the present invention have complex viscosities of at least 2�105 poise (P), preferably about 1�107 or more, where complex viscosity is measured by subjecting a sample to oscillatory shear at a fixed frequency of 0.1 rad/sec at 25� C. using a Rheometric Fluids Spectrometer� measuring films having a thickness of about 1 millimeter. The resulting viscous and elastic force responses are combined to determine the complex modulus which is divided by the imposed frequency to compute the complex viscosity.
A preferred siloxane gum is a diphenyl-dimethyl polysiloxane gum useful in the invention has a molecular weight of at least about 500,000, and must be diphenyl substituted to the extent of 3% or more, preferably at least about 5%. The siloxane gums are filler reinforced to provide additional rigidity. Silica is the preferred filler and is used at a level of from about 0.02% to about 2.00%.
Silicone resins are silicone polymers with a high degree of crosslinking introduced through the use of trifunctional and tetrafunctional silanes. Typical silanes used in the manufacture of resins are monomethyl, dimethyl, monophenyl, diphenyl, methylphenyl, monovinyl, and methylvinyl chlorosilanes, together with tetrachlorosilane. A preferred resin is one offered by General Electric as GE SR545. This resin is provided as a solution in toluene which is stripped prior to the resin's use.
The surfactant used in the present invention to premix with the rigid silicone is an alkyl glyceryl sulfonate. This material, used at a level of from about 0.2% to about 12% of an aqueous paste containing about 50% water, provides for the rigid silicone to be dispersed into small droplets and distribute better onto the hair. The alkyl group associated with the surfactant generally has from about 10 to about 20 carbon atoms, preferably from about 12 to about 14.
The compositions of the invention comprise a volatile carrier, or mixtures thereof, which preferably is present from about 0.1% to about 10%. The term "volatile" as used herein means that the material has a measurable vapor pressure.
Where the rigid silicone polymer is a polydimethyl siloxane or a polydiphenyldimethyl siloxane, the preferred carriers are volatile silicones having a boiling point between 99� C. to about 260� C. and have a solubility in water of less than about 0.1%. The degree of substitution on the siloxane (higher substitution, lower solubility) obviously affects the polymer's solubility and is taken into account by the formulator. The silicones may be either cyclic or linear polydimethyl siloxanes. The number of silicon atoms in the cyclic silicones is about 3 to about 7, most preferably 4 or 5. The general formula for the cyclic silicones is: ##STR1## wherein n=3-7. Viscosities are generally less than 10 centipoise (cP) at 25� C.
Linear polydimethyl siloxanes useful in the invention generally have viscosities of less than about 5cP at 25� C. The linear volatile silicones contain from about 3 to about 9 silicone atoms and have the general formula
(CH3)3 Si--O--[Si (CH3)2 O]n Si (CH3)3
wherein n=1-7.
Silicones of the above described types are widely available e.g., from Dow Corning as 344,345 and 200 fluids; Union Carbide as Silicone 7202 and 7158, and Stauffer Chemical as SWS-03314.
Also useful in compositions of the invention are certain volatile hydrocarbons. These hydrocarbons may be either straight chain or branched, and contain from about 10 to about 16 carbon atoms, preferably from about 12 to about 16 carbon atoms.
Short chain alcohols such as ethanol are also suitable solvents for use in the present compositions.
The surfactants useful in the shampoo compositions of this invention can be present at a level of from about 10% to about 30%, most preferably from about 12% to about 25% of the composition. Surfactants useful in compositions of the invention include anionic, nonionic, cationic, zwitterionic and amphoteric surfactants.
Synthetic anionic detergents useful herein, particularly for the shampoo compositions, include alkyl and alkyl ether sulfates. These materials have the respective formulae ROSO3 M and RO(C2 H4 O)x SO3 M where R is alkyl or alkenyl of about 10 to about 20 carbon atoms, x is 1 to 10, and M is a water-soluble cation such as ammonium, sodium, potassium and triethanolamine. The alkyl ether sulfates useful in the present invention are condensation products of ethylene oxide and monohydric alcohols having about 10 to about 20 carbon atoms. Preferably, R has 12 to 18 carbon atoms in both the alkyl and alkyl ether sulfates. The alcohols can be derived from fats, e.g., coconut oil or tallow, or can be synthetic. Lauryl alcohol and straight chain alcohols derived from coconut oil are preferred herein. Such alcohols are reacted with 1 to 10, and especially 3, molar proportions of ethylene oxide and the resulting mixture of molecular species, having, for example, an average of 3 moles of ethylene oxide per mole of alcohol, is sulfated and neutralized.
Specific examples of alkyl ether sulfates of the present invention are sodium coconut alkyl triethylene glycol ether sulfate; lithium tallow alkyl triethylene glycol ether sulfate; and sodium tallow alkyl hexaoxyethylene sulfate. Highly preferred alkyl ether sulfates are those comprising a mixture of individual compounds, said mixture having an average alkyl chain length of from about 12 to 16 carbon atoms and an average degree of ethoxylation of from about 1 to 4 moles of ethylene oxide. Such a mixture also comprises from about 0 to 20% by weight C12-13 compounds; from 60 to 100% by weight of C14-15-16 compounds, from about 0 to 20% by weight of C17-18-19 compounds; from about 3 to 30% by weight of compounds having a degree of ethoxylation of 0; from about 45 to 90% by weight of compounds having a degree of ethoxylation of from 1 to 4; from about 10 to 25% by weight of compounds having a degree of ethoxylation of from 4 to 8; and from about 0.1 to 15% by weight of compounds having a degree of ethoxylation greater than 8.
Another suitable class of anionic surfactants are the watersoluble salts of the organic, sulfuric acid reaction products of the general formula:
wherein R1 is chosen from the group consisting of a straight or branched chain, saturated aliphatic hydrocarbon radical having from 8 to 24, preferably 12 to 18, carbon atoms; and M is a cation. Important examples are the salts of an organic sulfuric acid reaction product of a hydrocarbon of the methane series, including iso-, neo-, ineso-, and n-paraffins, having 8 to 24 carbon atoms, preferably 12 to 18 carbon atoms and a sulfonating agent e.g., SO3, H2 SO4, oleum, obtained according to known sulfonation methods, including bleaching and hydrolysis. Preferred are alkali metal and ammonium sulfonated C12-18- n-paraffins.
Additional examples of anionic synthetic detergents which come within the terms of the present invention are the reaction products of fatty acids esterified with isethionic acid and neutralized with sodium hydroxide where, for example, the fatty acids are derived from coconut oil; sodium or potassium salts of fatty acid amines of methyl tauride in which the fatty acids, or example, are derived from coconut oil. Other anionic synthetic detergents of this variety are set forth in U.S. Pat. Nos. 2,486,921; 2,486,922; and 2,396,278.
Still other anionic synthetic detergents include the class designated as succinamates. This class includes such surface active agents as disodium N-octadecylsulfosuccinamate; tetrasodium N-(1,2-dicarboxyethyl)-N-octadecylsulfo-succinamate; diamyl ester of sodium sulfosuccinic acid; dihexyl ester of sodium sulfosuccinic acid; dioctyl esters of sodium sulfosuccinic acid.
Other suitable anionic detergents utilizable herein are olefin sulfonates having about 12 to about 24 carbon atoms. The term "olefin sulfonates" is used herein to mean compounds which can be produced by the sulfonation of α-olefins by means of uncomplexed sulfur trioxide, followed by neutralization of the acid reaction mixture in conditions such that any sultones which have been formed in the reaction are hydrolyzed to give the corresponding hydroxy-alkanesulfonates. The sulfur trioxide can be liquid or gaseous, and is usually, but not necessarily, diluted by inert diluents, for example by liquid SO2, chlorinated hydrocarbons, etc., when used in the liquid form, or by air, nitrogen, gaseous SO2, etc., when used in the gaseous form.
The α-olefins from which the olefin sulfonates are derived are mono-olefins having 12 to 24 carbon atoms, preferably 14 to 16 carbon atoms. Preferably, they are straight chain olefins. Examples of suitable 1-olefins include 1-dodecene; 1-tetradecene; 1-hexadecene; 1-octadecene; 1-eicosene and 1-tetracosene.
In addition to the true alkene sulfonates and a proportion of hydroxy-alkanesulfonates, the olefin sulfonates can contain minor amounts of other materials, such as alkene disulfonates depending upon the reaction conditions, proportion of reactants, the nature of the starting olefins and impurities in the olefin stock and side reactions during the sulfonation process.
The α-olefins from which the olefin sulfonates are derived are mono-olefins having 12 to 24 carbon atoms, preferably 14 to 16 carbon atoms. Preferably, they are straight chain olefins. Examples of suitable 1-olefins include 1-dodecene; 1-tetradecene; 1-hexadecene; 1-octadecene; 1-eicosene and 1-tetracosene.
In addition to the true alkene sulfonates and a proportion of hydroxy-alkanesulfonates, the olefin sulfonates can contain minor amounts of other materials, such as alkene disulfonates depending upon the reaction conditions, proportion of reactants, the nature of the starting olefins and impurities in the olefin stock and side reactions during the sulfonation process.
A specific α-olefin sulfonate mixture of the above type is described more fully in the U.S. Pat. No. 3,332,880 of Phillip F. Pflaumer and Adrian Kessler, issued July 25, 1967, titled "Detergent Composition", the disclosure of which is incorporated herein by reference.
Another class of anionic organic detergents are the beta-alkyloxy alkane sulfonates. There compounds have the following formula: ##STR2## where R1 is a straight chain alkyl group having from 6 to 20 carbon atoms, R2 is a lower alkyl group having from 1 (preferred) to 3 carbon atoms, and M is a water-soluble cation as hereinbefore described.
Specific examples of β-alkyloxy-alkane-1-sulfonates, or alternatively 2-alkyloxy-alkane-1-sulfonates, having low hardness (calcium ion) sensitivity useful herein to provide superior cleaning levels under household washing conditions include:
potassium-β-methoxydecanesulfonate, sodium 2-methoxytridecanesulfonate, potassium 2-ethoxytetradecylsulfonate, sodium 2-isopropoxyhexadecylsulfonate, lithium 2-t-butoxytetradecylsulfonate, sodium β-methoxyoctadecylsulfonate, and ammonium β-n-propoxydodecylsulfonate.
Many additional nonsoap synthetic anionic surfactants are described in McCUTCHEON'S, DETERGENTS AND EMULSIFIERS, 1984 ANNUAL, published by Allured Publishing Corporation, which is incorporated herein by reference. Also, U.S. Pat. No. 3,929,678, to Laughlin et al., issued Dec. 30, 1975 discloses many other anionic as well as other surfactant types and is incorporated herein by reference.
Nonionic surfactants, which are preferably used in combination with an anionic, amphoteric or zwitterionic surfactant, can be broadly defined as compounds produced by the condensation of alkylene oxide groups (hydrolphilic nature) with an organic hydrophobic compound, which may be aliphatic or alkyl aromatic in nature. Examples of preferred classes of nonionic surfactants are:
1. The polyethylene oxide condensates of alkyl phenols, e.g., the condensation products of alkyl phenols having an alkyl group containing from about 6 to 12 carbon atoms in either a straight chain or branched chain configuration, with ethylene oxide, the said ethylene oxide being present in amounts equal to 10 to 60 moles of ethylene oxide per mole of alkyl phenol. The alkyl substituent in such compounds may be derived from polymerized propylene, diisobutylene, octane, or nonane, for example.
2. Those derived from the condensation of ethylene oxide with the product resulting from the reaction of propylene oxide and ethylene diamine products which may be varied in composition depending upon the balance between the hydrophobic and hydrophilic elements which is desired. For example, compounds containing from about 40% to about 80% polyoxyethylene by weight and having a molecular weight of from about 5,000 to about 11,000 resulting from the reaction of ethylene oxide groups with a hydrophobic base constituted of the reaction product of ethylene diamine and excess propylene oxide, said base having a molecular weight of the order of 2,500 to 3,000, are satisfactory.
3. The condensation product of aliphatic alcohols having from 8 to 18 carbon atoms, in either straight chain or branched chain configuration, with ethylene oxide, e.g., a coconut alcohol ethylene oxide condensate having from 10 to 30 moles of ethylene oxide per mole of coconut alcohol, the coconut alcohol fraction having from 10 to 14 carbon atoms.
4. Long chain tertiary amine oxides corresponding to the following general formula:
wherein R1 contains an alkyl, alkenyl or monohydroxy alkyl radical of from about 8 to about 18 carbon atoms, from 0 to about 10 ethylene oxide moieties, and from 0 to 1 glyceryl moiety, and R2 and R3 contain from 1 to about 3 carbon atoms and from 0 to about 1 hydroxy group, e.g., methyl, ethyl, propyl, hydroxy ethyl, or hydroxy propyl radicals. The arrow in the formula is a conventional representation of a semipolar bond. Examples of amine oxides suitable for use in this invention include dimethyldodecylamine oxide, oleyldi(2-hydroxyethyl) amine oxide, dimethlyoctylamine oxide, dimethyl-decylamine oxide, dimethyltetradecylamine oxide, 3,6,9-trioxaheptadecyldiethylamine oxide, di(2-hydroxyethyl)-tetradecylamine oxide, 2-dode-coxyethyldimethylamine oxide, 3-dodecoxy-2-hydroxypropyldi(3-hydroxypropyl)amine oxide, dimethylhexadecylamine oxide.
5. Long chain tertiary phosphine oxides corresponding to the following general formula:
wherein R contains an alkyl, alkenyl or monohydroxyalkyl radical ranging from 8 to 18 carbon atoms in chain length, from 0 to about 10 ethylene oxide moieties and from 0 to 1 glyceryl moiety and R' and R" are each alkyl or monohydroxyalkyl groups containing from 1 to 3 carbon atoms. The arrow in the formula is a conventional representation of a semipolar bond. Examples of suitable phosphine oxides are: dodecyldimethylphosphine oxide, tetradecyldimethylphosphine oxide, tetradecylmethylethylphosphine oxide, 3,6,9,-trioxaoctadecyldimethylphosphine oxide, cetyldimethylphosphine oxide, 3-dodecoxy-2-hydroxypropyldi(2-hydroxyethyl) phosphine oxide, stearyldimethylphosphine oxide, cetylethylpropylphosphine oxide, oleyldiethylphosphine oxide, dodecyldiethylphosphine oxide, tetradecyldiethylphosphine oxide, dodecyldipropylphosphine oxide, dodecyldi(hydroxymethyl)phosphine oxide, dodecyldi(2-hydroxyethyl)phosphine oxide, tetradecylmethyl-2-hydroxypropylphosphine oxide, oleyldimethylphosphine oxide, 2-hydroxydodecyldimethylphosphine oxide.
6. Long chain dialkyl sulfoxides containing one short chain alkyl or hydroxy alkyl radical of 1 to about 3 carbon atoms (usually methyl) and one long hydrophobic chain which contain alkyl, alkenyl, hydroxy alkyl, or keto alkyl radicals containing from about 8 to about 20 carbon atoms, from 0 to about 10 ethylene oxide moieties and from 0 to 1 glyceryl moiety. Examples include: octadecyl methyl sulfoxide, 2-ketotridecyl methyl sulfoxide, 3,6,9-trioxaoctadecyl 2-hydroxyethyl sulfoxide, dodecyl methyl sulfoxide, oleyl 3-hydroxpyropyl sulfoxide, tetradecyl methyl sulfoxide, 3-methoxytridecyl methyl sulfoxide, 3-hydroxytridecyl methyl sulfoxide, 3-hydroxy-4-dodecoxybutyl methyl sulfoxide.
Zwitterionic surfactants, useful in shampoos, can be exemplified by those which can be broadly described as derivatives of aliphatic quaternary ammonium, phosphonium, and sulfonium compounds, in which the aliphatic radicals can be straight chain or branched, and wherein one of the aliphatic substituents contains from about 8 to 18 carbon atoms and one contains an anionic water-solubilizing group, e.g., carboxy, sulfonate, sulfate, phosphate, or phosphonate. A general formula for these compounds is: ##STR3## wherein R2 contains an alkyl, alkenyl, or hydroxy alkyl radical of from about 8 to about 18 carbon atoms, from 0 to about 10 ethylene oxide moieties and from 0 to 1 glyceryl moiety; Y is selected from the group consisting of nitrogen, phosphorus, and sulfur atoms; R3 is an alkyl or monohydroxyalkyl group containing 1 to about 3 carbon atoms; X is 1 when Y is a sulfur atom and 2 when Y is a nitrogen or phosphorus atom; R4 is an alkylene or hydroxyalkylene of from 1 to about 4 carbon atoms and Z is a radical selected from the group consisting of carboxylate, sulfonate, sulfate, phosphonate, and phosphate groups.
Examples include:
5-[S-3-hydroxypropyl-S-hexadecylsulfonio]-3-hydroxypentane-1-sulfate; p0 3-[P,P-diethyl-P-3,6,9-trioxatetradexocylphosphonio]-2-hydroxypropane-1-phosphate;
3-[P,P-dimethyl-P-dodecylphosphonio]-propane-1-phosphate; and
Other zwitterionics such as betaines are also useful in the present invention. Examples of betaines useful herein include the high alkyl betaines such as coco dimethyl carboxymethyl betaine, lauryl dimethyl carboxymethyl betaine, lauryl dimethyl alphacarboxy-ethyl betaine, cetyl dimethyl carboxymethyl betaine, lauryl bis-(2-hydroxy-ethyl) carboxy methyl betaine, stearyl bis-(2-hydroxy-propyl) carboxymethyl betaine, oleyl dimethyl gamma-carboxypropyl betaine, lauryl bis-(2-hydroxypropyl) alpha-carboxyethyl betaine, etc. The sulfobetaines may be represented by coco dimethyl sulfopropyl betaine, stearyl dimethyl sulfopropyl betaine, lauryl dimethyl sulfoethyl betaine, lauryl bis-(2-hydroxy-ethyl) sulfopropyl betaine and the like; amido betaines and amidosulfobetaines, wherein the RCONH(CH2)3 radical is attached to the nitrogen atom of the betaine are also useful in this invention. The amido betaines are preferred for use in some of the compositions of this invention.
Examples of amphoteric surfactants which can be used in the compositions of the present invention are those which can be broadly described as derivatives of aliphatic secondary and tertiary amines in which the aliphatic radical can be straight chain or branched and wherein one of the aliphatic substituents contains from about 8 to about 18 carbon atoms and one contains an anionic water solubilizing group, e.g., carboxy, sulfonate, sulfate, phosphate, or phosphonate. Examples of compounds falling within this definition are sodium 3-dodecyl-aminopropionate, sodium 3-dodecylaminopropane sulfonate, N-alkyltaurines such as the one prepared by reacting dodecylamine with sodium isethionate according to the teaching of U.S. Pat. No. 2,658,072, N-higher alkyl aspartic acids such as those produced according to the teaching of U.S. Pat. No. 2,438,091, and the products sold under the trade name "Miranol" and described in U.S. Pat. No. 2,528,378.
The above-mentioned surfactants can be used alone or in combination in the hair care compositions of the present invention. The alkyl sulfates, the ethoxylated alkyl sulfates and mixtures thereof are preferred for use herein.
Water is the last essential component of the present invention's compositions and generally comprises from about 40% to about 90% of the total composition.
Optional Components
The present shampoo compositions herein can contain a variety of other optional components suitable for rendering such compositions more acceptable. Such conventional optional ingredients are well known to those skilled in the art, e.g., pearlescent aids such as ethylene glycol distearate; preservatives such as benzyl alcohol, ethyl paraben, propyl paraben and imidazolidinyl urea; thickeners and viscosity modifiers such as a diethanolamide of a long chain fatty acid (e.g., PEG 3 lauric diethanolamide), cocomonoethanol amide, dimethicone copolyols, guar gum, methyl cellulose starches and starch derivatives, fatty alcohols such as cetearyl alcohol, sodium chloride, sodium sulfate, polyvinyl alcohol, and ethyl alcohol; pH adjusting agents such as citric acid, sodium citrate, succinic acid, phosphoric acid, sodium hydroxide, sodium carbonate, etc.; coloring agents such as any of the FD&C or D&C dyes; hair oxidizing (bleaching) agents such as hydrogen peroxide, perborate and persulfate salts; hair reducing agents such as the thioglycolates; perfumes; and, sequestering agents such as disodium ethylenediamine tetraacetate, polymer plasticizing agents such as glycerin and propylene glycol. Such agents generally are used individually at a level of from about 0.01% to about 10%, preferably from about 0.05% to about 5.0% by weight of the composition.
The pH of the present compositions is not critical and may be in the range of from about 3 to about 10.
As with all compositions, the present compositions should not contain components which unduly interfere with the performance of the compositions.
Methods of manufacture of the present shampoo compositions are described in the following examples.
The present compositions are used in a conventional manner.
The following Examples further illustrate the preferred embodiments within the scope of the present invention. The Examples are given solely for the purposes of illustration and are not to be construed as limitations of the present invention as many variations of the invention are possible without departing from its spirit and scope.
The following examples are representative of the present invention.
______________________________________ Weight %Component I II III IV______________________________________Ammonium Lauryl Sulfate 12.810 12.810 14.000 13.500Ammonium Laureth Sulfate 9.095 9.095 0.000 4.000Alkyl Glycereth Sulfonate 1.256 2.512 9.000 2.177Ammonium Xylene Sulfonate 0.010 0.000 0.000 0.750Dimethicone Gum*1 1.000 2.000 4.500 2.000Silica2 0.128 0.256 1.125 0.353Cyclomethicone 1.000 2.000 4.500 2.000Coco Diethanol Amide 2.300 2.300 0.000 0.000EDTA 0.100 0.100 0.000 0.000Monosodium Phosphate 0.500 0.500 0.000 0.000Disodium Phosphate 0.380 0.380 0.000 0.000Salt 2.000 2.500 0.000 0.000Perfume 0.500 0.500 1.200 1.200Preservative 0.033 0.033 0.033 0.033Coco Monoethanol Amide 0.000 0.000 3.000 4.000Ethylene Glycol Stearate 0.000 0.000 2.000 2.000Cetearyl Alcohol 0.000 0.000 0.600 1.000Sodium Citrate 0.000 0.000 0.050 0.050Citric Acid 0.000 0.000 0.050 0.050Sodium Hydroxide 0.000 0.000 0.010 0.027Sodium Chloride 0.000 0.000 1.700 1.000Water Q.S. Q.S. Q.S. Q.S.______________________________________ 1 SE30 or SE76 Gum, General Electric 2 Cabo-sil HS5, Cabot Corporation
The alkyl glycereth sulfonate (AGS) paste and rigid silicone/silica blend are mixed together at high shear in a ribbon mixer or comparable agitator for about 1-5 hours. At the end of this step, the mixture is a thick surfactant paste premix with finely dispersed silicone particles throughout the blend.
The paste premix is diluted with the water or surfactant solution diluent to form a lower viscosity silicone premix. This dilution takes place by mixing the materials with a ribbon mixer, agitator, blender, or other common mixing equipment. The concentration of the paste premix in the water or diluent can be from about 10 to about 90% of the total mix.
The diluted silicone premix can be added to an anionic surfactant shampoo base formula to disperse the silicones in a product base. This addition occurs at low to moderate agitation between about 70� and about 160� F.
The above described compositions all provide excellent hair condition and hair styling properties.
|Cited Patent
|Filing date
|Publication date
|Jul 24, 1963
|Jun 13, 1967
|Bayer Ag
|Stabilized self-emulsifying solutions of alkyl poly-siloxanes containing hydrogen linked with silicon
|Mar 15, 1971
|Aug 1, 1972
|Corning Glass Works
|Surface conditioner for glass-ceramics
|Oct 31, 1984
|Dec 17, 1985
|Dow Corning Corporation
|Conditioning shampoo containing amine functional polydiorganosiloxane
|Jul 10, 1985
|Nov 3, 1987
|The Procter & Gamble Company
|Shampoo compositions
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|Mar 1, 1988
|The Proctor & Gamble Company
|Process for making a silicone-containing shampoo
|Title not available
|Title not available
|Title not available
|Citing Patent
|Filing date
|Publication date
|Oct 31, 1989
|Jan 8, 1991
|The Procter & Gamble Company
|Silicone hairspray compositions
|Oct 31, 1989
|Jan 8, 1991
|The Procter & Gamble Company
|Hair care compositions
|Oct 31, 1989
|Jan 8, 1991
|The Procter & Gamble Company
|Silicone hairspray compositions
|Apr 9, 1990
|Mar 5, 1991
|Colgate-Palmolive Company
|Hair conditioning shampoo containing C6 -C10 alkyl sulfate or alkyl alkoxy sulfate
|May 1, 1990
|Mar 31, 1992
|The Procter & Gamble Company
|Clean conditioning compositions for hair
|Nov 16, 1990
|Oct 13, 1992
|The Procter & Gamble Company
|Mild skin cleansing toilet bar with silicone skin mildness/moisturizing aid
|Feb 11, 1992
|Mar 30, 1993
|Amway Corporation
|Conditioning shampoo
|Apr 9, 1990
|May 25, 1993
|Colgate-Palmolive Company
|Hair conditioning shampoo containing long chain alcohol component
|Jan 10, 1992
|Sep 14, 1993
|The Procter & Gamble Company
|Colorless detergent compositions with enhanced stability
|May 19, 1993
|May 10, 1994
|Colgate-Palmolive Company
|Mild personal cleansing compositions containing sodium alcohol ethoxy glyceryl sulfonate
|Dec 3, 1992
|Sep 13, 1994
|Colgate-Palmolive Company
|Hair conditioning shampoo containing long chain alcohol component
|Jul 6, 1994
|Nov 14, 1995
|Kao Corporation
|Liquid detergent composition
|Aug 9, 1994
|Jun 25, 1996
|Henkel Corporation
|Liquid pearlizing composition
|Jan 18, 1994
|Jul 16, 1996
|Composition for washing keratinous materials in particular hair and/or skin
|Jun 28, 1994
|Sep 10, 1996
|Ici Americas Inc.
|Conditioning shampoo containing insoluble, nonvolatile silicone
|Feb 13, 1995
|Nov 12, 1996
|Procter & Gamble
|Shampoo compositions with silicone and cationic organic polymeric conditioning agents
|Aug 24, 1994
|Mar 4, 1997
|The Procter & Gamble Company
|Mild shower gel composition comprising unique thickener system which imparts improved lathering properties and modified rinse feel
|Aug 24, 1994
|May 27, 1997
|The Procter & Gamble Company
|Mild shower gel composition comprising fatty alcohol which imparts improved lathering and thickening properties
|Sep 30, 1996
|Oct 7, 1997
|The Procter & Gamble Company
|Shelf stable skin cleansing liquid with gel forming polymer, lipid and crystalline ethylene glycol fatty acid ester
|Feb 22, 1995
|Jan 20, 1998
|The Procter & Gamble Company
|Hair conditioning compositions with silicone conditioning agent containing silicone resin
|Feb 8, 1995
|Feb 3, 1998
|The Procter & Gamble Company
|Shampoo compositions with silicone and cationic surfactant conditioning agents
|Jan 21, 1997
|Jul 28, 1998
|The Procter & Gamble Company
|Personal cleansing compositions
|Oct 28, 1996
|Feb 9, 1999
|The Procter & Gamble Company
|Shelf stable skin cleansing liquid with gel forming polymer and lipid
|Oct 2, 1996
|Mar 16, 1999
|The Procter & Gamble Company
|Three in one ultra mild lathering antibacterial liquid personal cleansing composition
|Dec 18, 1997
|Nov 9, 1999
|General Electric Company
|Silicone composition for bar soap applications
|Jul 26, 1999
|Apr 18, 2000
|General Electric Company
|Silicone composition for bar soap applications
|May 21, 1998
|Aug 1, 2000
|The Procter & Gamble Company
|Personal cleansing compositions providing improved hair and skin conditioning
|Jan 5, 2000
|Mar 6, 2001
|General Electric Company
|Silicone composition for bar soap applications
|May 12, 1999
|Mar 12, 2002
|Unilever Home & Personal Care Usa, Division Of Conopco, Inc.
|Hair care compositions and method for depositing swollen polymer particles onto hair
|Jun 5, 1998
|Aug 13, 2002
|Helene Curtis, Inc.
|Hair care compositions which provide hair body and which comprise elastomeric resinous materials
|Jun 18, 2002
|Nov 26, 2002
|Carlos A. Khantzis
|Apparatus for and method of producing liquid to clean and coat surfaces
|Dec 21, 2001
|Aug 5, 2003
|Unilever Home & Personal Care Usa Division Of Conopco, Inc.
|Hair care compositions and method for depositing swollen polymer particles onto hair
|Mar 13, 2001
|Oct 26, 2004
|Johnson & Johnson Consumer Companies, Inc.
|Conditioning compositions
|Jul 21, 2003
|Jan 27, 2005
|Librizzi Joseph J.
|Conditioning detergent compositions
|Sep 1, 2004
|May 12, 2005
|Nathalie Mougin
|Block ethylenic copolymers comprising a vinyllactam block, cosmetic compositions containing them and cosmetic use of these copolymers
|Sep 15, 2004
|Oct 27, 2005
|Nathalie Mougin
|Block ethylenic copolymers comprising a vinyllactam block, cosmetic or pharmaceutical compositions comprising them and cosmetic use of these copolymers
|Jun 2, 2005
|Apr 27, 2006
|Nathalie Mougin
|Block ethylenic copolymers comprising a vinyllactam block, cosmetic or pharmaceutical compositions containing them and cosmetic use of these copolymers
|Apr 21, 1993
|Dec 22, 1993
|Unilever Plc
|Cosmetic emulsion containing a resin material and process for making it
|Apr 7, 1994
|Oct 27, 1994
|Henkel Corporation
|Liquid pearlizing composition
|Aug 22, 1996
|Mar 6, 1997
|The Procter & Gamble Company
|High lather styling shampoos
|U.S. Classification
|424/70.12, 424/70.31, 510/122, 510/127, 424/70.21, 424/70.22, 424/70.24
|International Classification
|Cooperative Classification
|European Classification
|Jul 2, 1987
Owner name: PROCTER & GAMBLE COMPANY, THE
Free format text: ASSIGNMENT OF ASSIGNORS INTEREST.;ASSIGNOR:VU, HOANG D.;REEL/FRAME:004736/0247
Effective date: 19870518
|Sep 24, 1992
|Fee payment
Year of fee payment: 4
|Feb 4, 1997
|Maintenance fee reminder mailed
|Jun 29, 1997
|Lapse for failure to pay maintenance fees
|Sep 9, 1997
|Expired due to failure to pay maintenance fee
Effective date: 19970702


text:
Today, Video Conferencing systems can go way beyond anything imagined by companies. More and more companies, both large and small, are looking into these systems as a necessary resource. One of the reasons why so many businesses are using this now is because it helps them save time and money. With a focus on increasing productivity and cost reduction, and a general reluctance to travel, have all contributed to a intensified awareness of the essentialness of video conferencing. Video Conferencing brings work back to the office instead of taking it elsewhere. This allows access to important people, tools, and resources that would normally take time and money to get to. If a company does not yet have Video Conferencing, it is really only a matter of time until they do. Here a few signs that Video conferencing is a must-have immediate next step:
There are many services out there like Internet chatting services such as Messenger or Skype for regular communication; however this is not Video conferencing. When a company is dealing with many top tier clients, then video conferencing provides a more comprehensive solution. The distinction lies in the fact that video conferencing allows several people to talk all at once. In contrast, Skype and similar programs usually allow just one-on-one conversations. Video conferencing is an ideal solution for businesses that need to talk to several people all at once.
A second reason you may need Video conferencing is to bring remote employees together for meetings. If a company has many remote employees it can be very costly to get everyone together with travel expenses. It is necessary to bring employees together for numerous reason; comradery, data collaboration, and to examine documents. Video Conferencing also has the ability to share files and information easily.
Another sign you may see that means you need Video Conferencing would be that you want to have the best communication possible. Enhanced communications leads to better decisions and improved results from those decisions. Video conferencing seems to be picking up where the telephone and email have left off. Conferencing and teamwork tools can help company's quickly resolve issues, help with customer demands and stay on top of competitors. So, the predicament is not whether or not to invest in conferencing and collaboration, but rather which types of Video Conferencing features make the most sense for your company.
Finally, you may have some of the equipment for Video Conferencing already. This puts one foot in the door with installation; especially if a company already has a conference room set up for Video Conferencing but wants to add desktops. However, to set up a new Video Conferencing system, special hardware installation is necessary. If there is already an office, any quiet room will suffice to host the camera. If an office is being built for a new company, consider making one room a conference room only. A high-speed Internet access is essential for video conferencing because of how the data must be sent. Again, most larger offices are already equipped with high speed internet and are ready for installation on that level.
Video conferencing makes the working world a smaller, more effective environment for doing business. That said, with so many options, it's hard to know which video vendor is best for you. And while Google inquiries, YouTube videos, and blog posts can certainly help you make the right decision, truth be told, they often require far too much of your time, effort and energy …. more
New advancements are also making video more beneficial to a greater range of business areas including marketing, HR, and internal operations. Many solutions are economical, easy to use, and very effective at making communication more personal. more
More and more businesses are investing in video conferencing. The business benefits of video conferencing are well-established, with more than 90% of businesses who regularly use video conferencing benefit from improvements in productivity, better teamwork, and reduced travel expenses. more
If you're in the market for a video conferencing system, you know that today's systems offer more features and functionality than ever. Unfortunately, figuring out what you need is also incredibly difficult. more
This guide is all about outlining the different ways that cloud video conferencing can solve your business problems without creating any headaches or breaking the bank. So go ahead—browse around and learn more about video conferencing in the cloud. more

subset: commoncrawl


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Summer - a wonderful time! Time long walks in the fresh air, fun and active games.
Along with the game on the walk you can practice and development of the child.
It will take the baby pleasure and benefit.
Mini-garden. Together with your child find a quiet place in thecourtyard, loosen and pour it. Vegetable garden stones or weave the fence of twigs. At the plant to flower and follow its growth. Polite weeds, timely watering. The child is the activity creates a positive attitude towards work, his values, he sees the results of their work. A child watches the growth process of the way from seed obtained plant studies be logical chain.
Cheerful arithmetic. Chalk paint on the pavement geometric shapes, learn through the concept of "multi-little", various shapes and colors.
- Draw a chalk on the pavement several identical objects. Count them and then sign next to them the correct number.
- The same vice versa. Draw a figure, and the child shall bring the corresponding number of pebbles.
- With figures make molds of sand, for example, three machines 2 and berries. Encourage your child to determine what more.
letters. Crayon - a great way to learn letters.
- Write large letters on the pavement, and the child let the colors in the space inside them.
- Start to write the letter, and let the kid tries to continue.
- You can ask the child to jump on the letters written at a certain distance from each other and to remember the words that begin with them.
- Form words from letters. The child must find on the pavement he needed letters and jump on them.
- Write a letter and the child let her know. Then picture the object or animal that begins with that letter.
- Let the kid looking for his familiar letters among many others.
Bryzgalki. When still play in the streets with water, but in the summer? Make bryzgalku from the bottle (you can buy ready-made water gun) and draw water on the sand.
Pebbles and sticks. From the materials at hand, you can add geometric shapes, count the pebbles, it is difficult in a row, decorate their figurines from sand.
Find object. Prepare home cards izborazheniem flowers, insects, objects (a bicycle, shovel, bucket). Together on the street looking for something that is shown in the picture.


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Pet Sitter in Toronto
I have a lot of experience in Dog Walking and also I am ready to take care of your pets at your home while you are out. I can deal with all kinds of personalities of dogs as I had a pet. Utmost care will be taken of your pets as I am a hardcore pet lover.
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Decorative coatings in Cebu
Found: 1 products← Back to category "Decorative coatings"
Wood coating finishing
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SPARKO offers a wide range of finishing products from surface coatings, Thinners & Solvents, Gold Leaf, Wood Glues, Abrasives and spray equipment. Read more
Philippines, Cebu
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Decorative Coatings
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Architectural and decorative coatings are used for interior and exterior architectural finishing. Products serve the requirements of housing, commercial and residential buildings, hotels and recreational facilities, and institutional accounts. The major products under this group are clear nitrocellu Read more
Delivery to Cebu fromTaytay
Davies Acreex Floor & Wall Coating
In stock
Chlorinated Rubber Based Floor & Wall Coating A modified chlorinated rubber-based coating formulated to protect and beautify floors, walls and roofs. It has outstanding exterior durability and abrasion resistance. It forms a tough, smooth, sheen finish with good alkali and chemical resistance. Read more
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Nickel Plating
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Nickel Plating The nickel plate is a hard protective layer, and is the foundation of a chrome plated item. It is the nickel you'll usually see peeling from an old bumper or tail-pipe of a motorcycle. As this is a hard metal, it is more difficult to polish or burnish, and so it is essential that all Read more
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Small Cap Quant - Stoneridge Investment Partners - Investment Styles
The StoneRidge Quantitative Small Cap Growth Equity portfolio seeks to outperform its benchmark (the Russell 2000 Growth index) and industry peers over a .
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A certain Jatto Abiodun Emmanuel, the lucky winner of the second edition of Infinity Mobility/Completesportsnigeria.com Hot Match Preview For Infinix Hot 4 Prize gleefully received his prize on Friday in Abuja.
In the pictures above, cheerful winner, Jatto (r), a Garki II Abuja resident, receives his Infinix Hot 4 prize sponsored by Infinix Mobility from Complete Sports' Abuja Correspondent, Richard Jideaka.
An elated Jatto told Completesportsnigeria.com, "I am so happy that the prize I won has become a reality – I have received this beautiful phone, Infinix Hot 4. I almost can't believe this is happening to me. Many thanks to Completesportsnigeria.com and Infinix Mobility, for making it a simple and credible competition."
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What years did the tv show : that 70s show: run on tv
kgb answers » Arts & Entertainment » TV » What years did the tv show : that 70s show: run on tv
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Mailbag: How will Schottenheimer use both Zac Stacy and Tre Mason? Will it be a two-headed monster like he ran in 2010 with Shonn Greene and LaDainian Tomlinson on the Jets? – Jacob, Prescott
Zac Stacy did exceptionally well for a rookie last year, even more impressive that he nearly topped 1,000 yards in just 12 starts. But he did amass a whopping 250 carries, which is way too many in 12 games, for any back.
The question isn't will there be a second back complimenting Stacy, but who will it be?
Tre Mason was obviously drafted for a reason. Coming from the ultra-competitive SEC, Mason is built for the fierce NFC West. But, Benny Cunningham, who was the Rams' no. 2 last year, will battle with Mason for that spot. I expect Mason though, to be listed as the no. 2 come Sept. 7.
Mason, at Auburn last year, racked up an astounding 1,816 yards on 317 carries (5.7 avg.), while scoring 23 touchdowns. The guy is durable, built like a fireplug and should fit in well with what Schottenheimer wants to do offensively, which is punish the opposing defensive front seven.
Jeff Fisher and co. will be keeping a keen eye on the backfield this preseason looking for a reliable backup who can step in and make an impact. Expect training camp and the first three preseason games to be fierce competitively as Mason, Cunningham, and perhaps even Isaiah Pead, battle for roster spots.
If it is indeed Stacy and Mason taking the bulk of the carries, then it's not outlandish to think that as a tandem, they can total 1800+ yards. Last year, the Rams ran a total of 373 times with running backs. I expect that number to increase this year now that their identity will be ground and pound from day one. Rushing for 450-500 times will not only allow the Rams to control the clock and the line of scrimmage, it will also take a lot of pressure off Sam Bradford.
One aspect to not overlook in the running back's potential success is the road graders they have in front of them: Roger Saffold, Greg Robinson, and Jake Long. If, and this is a big if, the line can stay healthy, expect this running back tandem to inflict some damage in 2014.
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text:
Business Improvement Techniques (Yellow Belt)Coaching For Change
£ 385 - (456 €)
Wichtige informationen
- Workshop
- Inhouse
- Manchester (Grossbritannien)
- Dauer:
2 Days
- Wann:
Freie Auswahl
Zu verbessern Everything good.
Kurs abgeschlossen: Mai 2015 | Recomendarías este centro? Sí.
Zu verbessern Nothing negative.
Kurs abgeschlossen: Februar 2015 | Recomendarías este centro? Sí.
Was lernen Sie in diesem Kurs?
Business Strategy
Business Analysis
Business Development
Strategic Management
Six Sigma
Strategic Planning
Business Plan
Stategy Management
Strategy Development
Lean Management
Sigma Certification
Business Improvement Techniques
Lean Six Sigma
Yellow Belt
Course review
This 2 day course is endorsed by the Institute of Leadership and Management. The ILM is the UK's leading provider of leadership, coaching and management qualifications and training. The course is designed to give individuals an insight into lean six sigma, process improvement tools. You will understand the role of a "Yellow Belt" in a project team led by a "Green Belt".
At the end of the training individuals will understand how they can support improvement projects, become more competitive and deliver bottom line savings. One client has trained 56 Managers and Directors investing £20k in this training and realised potential returns of £214k.
What's the format of the course?
You will:
- Gain an understanding of how Lean and Six Sigma fit together and be able to articulate this with co-workers.
- Understand the 7 wastes and the impact on performance by focusing on them.
- Understand the DMAIC approach and the need for a data driven approach to problem solving to ensure problems dont come back.
- Have an awareness of the 7 quality tools, when and how to use them.
- Understand the difference between containment and countermeasure and some lean tools that can be used to expose and address abnormalities.
- Be in a position to challenge waste in your business.
- Understand the principle of VOC (voice of the customer) and links to CTQ (critical to quality measures).
- Have the tools to tackle a problem in a systematic way.
- Understand leadership roles needed in the pursuit of a continuous improvement culture.
Zusätzliche Informationen
Stimmt etwas nicht mit diesem Kurs? Informieren Sie uns wenn Sie einen Fehler entdecken und helfen somit auch anderen Usern wie Sie.


text: So I found this checker and tested it out, works pretty well and accurate. Virustotal shows 8 detections so download at your own risk, will post original source from github too so please don't accuse me for not putting up warnings. It's been on my PC for 2 weeks now and I have proof it works. Hidden Content: You must 'reply' before you can see the hidden content. Virustotal: https://www.virustotal.com/en/file/...bcd28f47e4763bcabe0f2bceba51936e0ee/analysis/ If you scan just the download link it'll show 0, the file downloaded shows 8. Like if you tried it out and worked Any other questions please ask


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Is Mr. Lube incorrect or missing key business information? Update your Hotfrog listing today.
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Hotfrog Canada provides information regarding Mr. Lube in Nepean ON. Mr. Lube is located at 1850 Robertson Rd, Nepean ON K2H 5B8 and provides Automotive services. Contact them on (613) 828-8171 or by visiting them on their website http://mrlube.com.
Opening hours
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Paper Doilies 5.5" Round 40/Pkg"Cake Decorating
White - View Complete Details
Product Number: NOTM404287
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Estimated Delivery - 15 business day(s) - Mon 3/20 16 business days - Mon 3/20
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Paper Doilies 5.5" Round 40/Pkg" - UNIQUE INDUSTRIES-Doilies. These paper doilies are white allowing you to creatively add your personality to them, or leave them white! This package includes forty doilies that measure 5-1/2 inches in diameter. Imported.View Product Specs
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This little angel was sent from above and you marvel at this daily. Show her that you think of her constantly and consider her your angel with our My little angel necklace. Her heart will have wings just like this precious treasure.
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Just what I expected - perfect gift for my little granddaughter.


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Opinie gości
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Located a 2-minute walk from Galerías Commercial Centre, this hotel offers free Wi-Fi and free parking in central Bogota. Continental breakfast is included. The rooms in Hotel Galerías Inn feature a private bathroom with hairdryer, safety deposit box, and LCD TV. There is a 24-hour front desk service. Continental breakfast includes coffee, toasts, cereal, jams, and juices. La Candelaria historic centre is a 15-minute drive from Hotel Galerías Inn, and Corferias Convention Centre is a 30-minute drive away.El Dorado Airport is a 30-minute drive away.


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7 CFR Part 770 - INDIAN TRIBAL LAND ACQUISITION LOANS
66 FR 1567, Jan. 9, 2001, unless otherwise noted.
Title 7 published on 2015-08-22
The following are ALL rules, proposed rules, and notices (chronologically) published in the Federal Register relating to 7 CFR Part 770 after this date.
Title 7 published on 2015-08-22.
The following are only the Rules published in the Federal Register after the published date of Title 7.
For a complete list of all Rules, Proposed Rules, and Notices view the Rulemaking tab.


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WIMBLEDON '11: Tournament at a glance
A look at Wimbledon, the year's third Grand Slam tennis tournament:
Surface: Grass courts.
Site: The All England Lawn Tennis and Croquet Club.
Schedule: Play begins Monday. The women's singles final is July 2; the men's singles final is July 3. There is no play scheduled for the two-week tournament's middle Sunday, June 26.
2010 Men's Singles Champion: Rafael Nadal of Spain.
2009 Women's Singles Champion: Serena Williams of the United States.
Last Year: Nadal beat Tomas Berdych of the Czech Republic 6-3, 7-5, 6-4 for his second Wimbledon title. Berdych had eliminated six-time champion Roger Federer in the quarterfinals. Williams won her fourth Wimbledon singles championship and 13th Grand Slam title overall by beating Vera Zvonareva 6-3, 6-2 in the final.
Key Statistic: 26-2 — Nadal's record at Wimbledon from 2006-10, reaching the final all four times he's entered the tournament in that span. He lost to Federer in the 2006 and 2007, then won the 2008 and 2010 championships; Nadal didn't play at Wimbledon in 2009 because of knee tendinitis.
Two Key Returns: The Williams sisters are entered in Wimbledon after lengthy injury absences. Serena missed nearly a full year before coming back at a grass-court tuneup tournament in Eastbourne, England, this month; Venus was out since January until returning at that same event. They have combined to win nine of the 11 Wimbledon women's singles titles since 2000.
When It Rains: As of 2009, Centre Court is fitted with a retractable roof, which allows matches to be played during wet weather.
New This Year: A plaque on Court 18 notes it was the site of the record-breaking, 11-hour, 5-minute first-round match last year between John Isner and Nicolas Mahut, which Isner won 70-68 in the fifth set.
Prize Money: Total is 14.6 million pounds (about $23.5 million), with 1.1 million pounds (about $1.77 million) each to the men's and women's singles champions.
Copyright 2011 The Associated Press. All rights reserved. This material may not be published, broadcast, rewritten or redistributed.


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Posted: Sunday, February 26, 2017 8:02 AM
Looking for the girl next door?? Or something a bit on the wild side? You can find it here :)
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School offers counseling for traumatized students who saw classmate chew breakfast pastry into shape of gun
**Written by Doug Powers
A Baltimore area elementary school recently suspended a seven year old boy for chewing a breakfast pastry into a shape resembling a gun. There also seems to be some dispute over whether the boy said "bang bang" after doing so (some also claim there might have been a second Pop-Tarter on the grassy knoll).
For any students who were traumatized by the frightening toaster strudel ordeal, counseling is available:
The school sent home a letter to parents saying, "During breakfast this morning, one of our students used food to make inappropriate gestures that disrupted the class. While no physical threats were made and no one was harmed, the student had to be removed from the classroom."
Parents should talk to their children if they're troubled by the incident, the school said, and the school counselor will be available for any student who needs to talk.
It's been pointed out that because the Pop Tart had a filling, the pastry weapon was likely considered to be loaded — a much more egregious zero-tolerance violation indeed — hence the suspension.
The letter sent to the parents of students is here. The educators will now undoubtedly insist that any Pop Tarts consumed on school property undergo a mandatory 24-hour cooling off period after coming out of the toaster.
Related: Hello Kitty Bubble Gunfight at the PC Corral
**Written by Doug Powers
Twitter @ThePowersThatBe
Texas college's suggested term for 'holiday party' COULD trigger accounting majors
December 14, 2016 04:12 PM by Doug Powers
Irony 101: Washington State U. profs WILL NOT TOLERATE free speech they consider intolerant
December 13, 2016 10:28 AM by Doug Powers
Perfect: Vermont's Burlington College feels the Bern
May 16, 2016 09:31 PM by Doug Powers
Full circle legacy: Former DHS director J-Nap doling out millions of taxpayer dollars to 'undocumented students' at UC
May 12, 2016 09:24 PM by Doug Powers
The trouble with Carly Fiorina: Top 11 red flags
April 28, 2016 12:14 AM by Michelle Malkin
Categories: 2016 Campaign, Education, Feature Story, Immigration


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Magic can be so many things to a child.
It can be the discovery of how bubbles burst the moment he touches them.
It can be the discovery of a new secret hiding place in his favorite playground.
It can be the discovery of how a caterpillar changes into a butterfly.
A book filled with a variety of ideas for parents to do with their toddlers age 0 – 24 months old, MindChamps Publishing's latest book Magic Moments: Small Beginnings is written by Carmee Lim and Brian Caswell.
The book introduces the concept of the '3 Minds' – the Champion, Learning and Creative mind, and touches on the importance of the environment and parent-child play. From activities to stimulate your infant's five senses, to indoor and outdoor activities, this book makes the perfect activity hand book for parents who are lost for ideas.
Based on years of research and practice, coupled with understanding of neuroscience and psychology of the learning brain, this book opens the door to parents on how parenting can be simple, fun and unintimidating.
What magic moments would you create with your child today?
Magic Moments: Small Beginnings is now available at MindChamps' Online Store.


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Taxation Principles and Concepts (Taxation)
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Taxation Principles and Concepts (Taxation) By Student's name Code+ course name Instructor's Name University Name City, State Date of Submission Taxation Principles and Concepts (Taxation) FIRST REQUIREMENT Dear Tobby, Hello, my friend. It has been a long time since we last met at campus…
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A capital allowance refers to the amounts in cash that a business operating in the United Kingdom can deduct from the overall income tax on its profits or the corporate tax. The sources of these sums of money come from certain purchases as well as investments as outlined in the Capital Allowances Act of 2001 (Channer & Rogers 2007, p.xiv). A business or corporate organization can claim capital allowances on the costs of cars, vans and machines purchased for business use, or other assets in the business such as scaffolding, equipment, ladders, furniture, computers, and tools. In addition, a business can also claim capital allowances on the expenditures incurred on plant and machinery, as well as, on facilities and equipment used for research and development, and items that a business operator uses privately before using them commercially. Another capital deduction occurs on the premises used for the company to run its business, such as improving a property, and converting a space above a building for rental purposes. As for your case Tobby, you can claim capital allowances on the following items: computers, car, premises and rent for Tamara. The capital allowance on computers is ? 200, car as ? 2,700, premises at ? 12, 5000 and Tamara's rent at ? 4,000. As such, the total capital allowance that Tobby can claim from the tax authority is ? 19,400 (Dunn & Rogers 2008, p.664). ...
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Back in 2002, the government introduced new reforms on company cars. The company car tax reform encourages people to buy of choose cars with lower levels of carbon dioxide (CO2) emissions. Purposely, the reforms are aimed at tackling changes in climate and greenhouse gas emissions. Also, it also encourages manufacturers to introduce greener cars. As a result, businesses should evaluate their…
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Rajasthan Online Scholarship Form 2015 | ROSE Online Application
Rajasthan State Scholarship online form is started on official site http://18.104.22.168/rajpms/ . government Deparrt of the The Social Justice & Empowerment invites notification for Post Metric Scholarship Scheme of Rajasthan / Uttar Matric Scholarship Scheme of Rajasthan / Samaj Kalyan Vibhag Scholarship Rajasthan for School & College
Follow the above step for the Rajasthan Online Scholarship Form 2015 . Right now Scholarship application submission for year 2014-15 has been stopped till further notice. Portal shall be opened for year 2015-16 in month of July, 2015.
Steps: Apply for Online Scholarship of Rajasthan
|· First Go on the "New Registration" Form and fill the provide desired details carefully and get Login ID and Password.keep safe the Registration ID/Login ID & Password if you are forget the password and ID then you have not registered again
Now login inside with ID/Password and click on the "Apply for Scholarship" button provides all desired details, check and after confirmation "Lock" the Application . For youre use Take print out the Application, get sign from your institution, attach all desired documents and send that to concerning Domicile District office by post.
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· Follow this links for the for the Rajasthan Online Scholarship Form 2015 http://18.104.22.168/rajpms/Document/User%20Manual-Out%20of%20State%20Students.pdf
Apply Online Rajasthan Online Scholarship Form 2015
You can check and apply Rajasthan scholarship form online from here:


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Feb 15, 2017
Demonetisation dole: How Mamata Banerjee is pushing West Bengal to precipice of fiscal disasterIn trying to score a goal against Modi's demonetisation, Mamata Banerjee has put the ball in her own net and set a dangerous precedent of recklessness.
Feb 14, 2017
Mamata Banerjee declares Kalimpong as separate district of West BengalA new district of Kalimpong was on Tuesday carved out of Darjeeling, which has seen separate statehood demands since 1980s, with Chief Minister Mamata Banerjee making the formal announcement here.
Feb 14, 2017
AIADMK crisis: Culture of authoritarianism when unchecked can destabilise even formidable political forcesThe messy leadership transition on display within the All India Anna Dravida Munnetra Khazagham (AIADMK) highlights the deeply flawed structure and functioning of the Indian political party system.
Feb 08, 2017
Chaos hits West Bengal Assembly over property bill; MLA Abdul Mannan injured in ruckusLeader of opposition and Congress MLA Abdul Mannan was admitted to hospital after being injured in a ruckus over Property Damage bill in the West Bengal Assembly. The ruckus started in the state Assembly after the opposition demanded more amendments in the bill.
Feb 02, 2017
Union Budget 2017: With token gestures for women, it is an average budget meant for a male audienceWhen the budget came out last year, we wondered what exactly Arun Jaitley and his Finance Ministry thought they were doing.
Feb 01, 2017
Budget 2017 is clueless, misleading, full of hollow words: Mamata BanerjeeTerming the Union Budget 2017 as "clueless and misleading", West Bengal Chief Minister Mamata Banerjee claimed it has no road map and is full of jugglery of numbers and hollow words.
Jan 30, 2017
Mamata Banerjee-led TMC to boycott first two days of Union Budget over protest against demonetisationTrinamool Congress chief Mamata Banerjee, who is angry over the arrest of its two MPs by CBI in connection with the chit fund scam, will not attend Parliament on 1 February when the Budget is presented.
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Jan 26, 2017
Victoria Memorial should be converted into a museum on British atrocities: TharoorPolitician and writer Shashi Tharoor has said the Victoria Memorial Hall in the metropolis should be converted into a museum on atrocities by the British during its rule in the country.
Jan 20, 2017
Finance Minister Arun Jaitley skips Bengal Global Business eventJaitley was scheduled to attend the event, but he was believed to have been asked by the party high command to stay away, according to sources.


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About Us
About Us
This website is a project of the Alice Paul Institute (API) in Mt. Laurel, NJ. It is written (except where otherwise noted) and administered by Roberta W. Francis, API ERA Education Consultant and Founding Chair (1999-2015), ERA Task Force, National Council of Women's Organizations.
We welcome emails to email@example.com.
To make a tax-deductible contribution in support of this website's educational mission, please contact API (856-231-1885, email@example.com) with credit-card information, or send a check (payable to "API – ERA") to Alice Paul Institute, P.O. Box 1376, Mount Laurel, NJ 08054.
The Alice Paul Institute, a not-for-profit corporation based at Paulsdale in Mount Laurel, NJ, was established in 1984 as the Alice Paul Centennial Foundation. This founding group of dedicated volunteers kept Alice Paul's papers intact after her death by purchasing them at auction and donating them to the Smithsonian Institution and Radcliffe College. They then took on the monumental challenge of buying and preserving Paulsdale, Alice Paul's birthplace. The API's principal mission is to increase public awareness of the life and work of Alice Paul (1885-1977), woman suffrage leader and author of the Equal Rights Amendment. The organization also promotes gender equality through programs for the education, development, and empowerment of young women leaders.


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Wednesday, August 26, 2015
6:38 AM Christian Lamitschka No comments
"There is a gag order, so I can't tell you no more," sings The Warden on "Salvation," one of the twelve tracks on his debut solo album, set for release on October 9, 2015 via Dallas, Texas indie label, Idol Records. "Salvation" is a story of touring the country in a struggling band, drinking way too much, and the glory of youth. One of the many honest, intriguing stories of The Warden's adventurous life, documented on his debut record.
"[The song 'Salvation'] allows me to relive my 20s," says The Warden, at a ripe 37 years of age. "I marvel about going on the road now, like I used to, when I was a teenager. That being said, when I was actually on the road, sleeping in a van, in January in a Home Depot parking lot, in Ypsilanti, Michigan, it wasn't necessarily living up to my expectations. 'Salvation' is a nice slice of nostalgia mixed with a little bit of a warning message."
Now, you're probably asking yourself, "who is The Warden?" He is East Dallas, Texas resident musician Ward Richmond, a fixture on the local scene who has toured internationally with projects such as Slick 57 and Boys Named Sue, among others, where he's held down the bass, songwriting, management duties, and sometimes vocals of these local music legends. This time, though, he's picking up the guitar and making all of the decisions by himself.
While still an active member of Dallas' country outfit Boys Named Sue (voted "Best Country Band" in Dallas, Texas - 2005, 2006, 2007, 2010), he ended up writing a handful of songs on his own, inspired by the birth of his daughter, Betty Sue, and recorded them with just his acoustic guitar on his iPhone. Eventually, he handed his tunes over to his longtime friend, and musical cohort, Robert Jason Vandygriff (from notable Dallas bands The Von Ehrics and RJV & Hell County Revival), and Jason talked him in to making a solo record.
"These songs are all pretty personal so I didn't really want to create an opportunity for three other dudes to modify songs that I was already perfectly content with," he says of his decision to make a solo record. "Boys Named Sue is a very collaborative effort and these weren't the right tunes for that project."
After about a week and a half of recording, at the legendary Echo Lab in Argyle, Texas (where Old 97's, Centromatic, Polyphonic Spree, and Slobberbone have worked), magic happened.
"It turned out better than I expected," he says with joy. "Jason had the vision and executed above all expectations."
Self-described as "East Dallas honky tonk," the record mixes foot-stompin' honky tonk and authentic, Texas-style storytelling with a slight dash of Southern punk rock, resulting in a countrified memoir looking back over the past fifteen years of The Warden's life, presenting tales of lifelong friendships, falling in and out of love, and the wild-ass adventure that happened along the way.
"It's pretty much lyric-driven," he comments. "Our goal was to up the quality of the music in order to kick a little extra ass, and add some excitement to the lyrics. Basically, it is a tonked up autobiography with a little fiction thrown in for good measure. It's much easier for me to approach it this way, as a tonk album - and probably more entertaining for others - than attempting to write an actual book."
He didn't do it by himself, though, which is something he wants to point out.
In addition to Vandygriff producing the record, and Echo Lab's Dave Willingham behind the boards, he enlisted the help of a blistering honky tonk orchestra made up of his friends (not to mention, some of the best damned talent the State of Texas has to offer), including Chad Stockslager (The Drams, The King Bucks, Hard Nights Day), Bruce Alford (Jack Ingram, 1100 Springs, Stoney LaRue), Dan Phillips (True Widow, Slowride, Reverend Horton Heat), and Burton Lee (1100 Springs, Mike & The Moonpies). He also convinced local stalwarts Madison King, Leslie McDonel (American Idiot), and John Pedigo (Slick 57, Boys Named Sue, The O's) to join him in the studio.
McDonel's gospel vocals make "County Line" come alive. A love song about new beginnings, it's rollicking rhythm section melds perfectly with The Warden and McDonel's hard-charging vocals. Meanwhile, the old Slick 57 punk tune, "Bullets," gets re-worked into a country duet, with The Warden and Madison King's voices melding into a warm, though still ragged, hungover, regretful number.
The album isn't all honky tonk, though. The Southern rock of "Little Darlin'" and the piano-filled, hometown anthem "Livin' In The EDT," gives you a taste of rock from the eyes of the South.
One thing is for sure; after listening to The Warden, you will want to live vicariously through the album again and give it another spin. Sit down and have a beer with The Warden and you'll likely hear tales about opening for Waylon Jennings, sneaking onto Willie Nelson's tour bus, and joining Billy Joe Shaver onstage to sing "Honky Tonk Heroes."
A true Texan, proudly born and raised in East Dallas (The EDT), this debut album is a testament to the fact that The Warden works hard each day at the art of livin' life properly.
Famed tattoo artist, and friend, Oliver Peck even designed the logo for the cover art. Originally, this album was not self-titled; yet, after seeing Peck's logo design for him, The Warden decided to just make the record self-titled.
"Oliver came up with a sweet logo, and I felt like it was good looking enough to ditch the album title," laughs The Warden.
As he sings in "High Life," "Miller High Life is the cure for when we are not sure of if we'll get some money in the bank," this record is the cure for anyone that doesn't feel like they're living life to the fullest. Put this on, get inspired, or just laugh and drink, and experience The Warden.
Remember, he's just an East Dallas boy that woke up one day and wrote a handful of songs to put a smile on your sweet mouth.
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Quote of the week
Now that Minnesota has legalized same-sex marriage, this anguished cry sounds even more so:
I don't know why gay people choose gayness, but I chose to be straight the day I realized "Although I never ever ever want children, I just adore the added fillip and excitement that 'risk of pregnancy' adds to my sex life. And when I was single and dating which is to say, spending time alone with people I didn't necessarily know very well I also loved that added risk of violent death vis-a-vis sexual dimorphism: if I'm with a woman who turns out to be a violent psycho hoping to kill me with her bare hands, there's a pretty decent chance I could successfully defend myself against her. Which is booooriiiiiing. Gimme a psycho attacker who outweighs me by at least a hundred testosterone-enriched pounds! And my chances of getting AIDS and other STDs were always a lot higher from straight sex, too. With all the kickass advantages heterohood has to offer childfree women like me, it's obvious that only a self-hating, risk-taking, masochistic fool of a woman would choose to be a lesbian instead."
As proposals go, this one is fairly modest; but 'tis enough, 'twill serve.


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Season 2 of the Overtime podcast is here! Listen to the first episode with Meg Robichaud now.
Tools section of my portfolio site. Http://www.scribbleandtweak.com I am looking to wrap this up this week, any criticism welcome.
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We used Ava Me photography to take photos for a company event at the Bong Bong Picnic Races. Joel was all over it! We asked for photos of everyone being natural and enjoying themselves and that's exactly what we got! Joel was able to capture the feel of the day perfectly! Gr..
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text:
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I am Chris Hardwick. I am on TV a lot and have a blog at nerdist.com. This podcast is basically just me talking about stuff and things with my two nerdy friends Jonah Ray and Matt Mira, and usually someone more famous than all of us. Occasionally we swear because that is fun. I hope you like it, but if you don't I'm sure you will not hesitate to unfurl your rage in the 'reviews' section because that's how the Internet works.
Parental Advisory
April 1st, 2011
Episode 78 of 855 episodes
Chris sees Anthony Michael Hall (in the hall), Jonah is slowly healing and Matt gets an inversion table.
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Welcome to the daily audio workout for your head.


text:
A New World History of Art.
CHENEY, Sheldon.
Place Published: New York
Date Published: 1956
Description: 8 color plates, and a profusion of b/w illus. 676pp. Short thick 4to, cloth, d.w. New York, 1956. A very good copy, signed by the author on half title page.Signed: Y
Binding: hardcover
Condition: very good
Language: English
Type: Books
Book ID: 107375
By This Author: CHENEY, Sheldon.