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Phase transitions in

Phase transitions in sintered ( were investigated by means of a differential scanning calorimeter (DSC) in combination with magnetization measurement. Below 300 K, three phase transitions were identified: charge disorder-order, paramagnetism-antiferromagnetism and antiferromagnetism-canted spin structure transitions. In contrast to the reported single-crystal sample, no field-induced metamagnetic transition occurred in the sintered sample at an applied magnetic field up to 6.5 T, and the resistivity of the sintered sample exhibited a semiconducting behaviour between 77 K and 300 K.