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New apparatus for ceramic texturing working under uniaxial stress and in a magnetic field

We have developed a new versatile apparatus combining the effect of hot pressing and the effect of magnetic field to texture HTSC (high-temperature superconductor) ceramics. The experimental set-up allows application of uniaxial stress up to 1100 degrees C under a maximum pressure of 60 MPa, in a controlled atmosphere and a magnetic field of 8 T. We have optimized the cycle for stress application along with the thermal cycle to produce highly-textured ceramics. In this paper, we describe the stress and thermal cycles used to texture Bi-Pb-Sr-Ca-Cu-O (2223 phase) ceramics. We present the physical and chemical characterizations of the samples which show a strong degree of crystallite orientation.