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The crystal structure of the monoclinic Fe2(SO4)3

The crystal structure of the monoclinic Fe2(S04)3 has been determined using three-dimensional intensities, measured with an automated Philips PW 1100 single-crystal diffractometer. The structure was essentially obtained from the three-dimensional Patterson synthesis by applying the minimum function. The cell constants, obtained by least-squares from direct O-value measurements on the diffractometer, are: a = 8.2955, b = 8.5332, c = 11.6304 A, fJ = 90.25 0; Z = 4; the space group is P 21/n. Atomic parameters and anisotropic temper-