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Nuclear Magnetic Resonance of 113Cd and 199Hg in Cd-Mg and Cd-Hg Solid Solutions.

The current theoretical and experimental situation with respect to Knight shifts and bulk susceptibility of Cd in pure Cd and in Cd-Mg and Cd-Hg alloys is reviewed. New experimental isotropic and anisotropic Knight shift data on 113Cd in Cd-Mg and Cd-Hg alloys and on 199Hg in Cd-Hg alloys are presented. The behavior of the 199Hg sites is found to be remarkably similar to that of the 113Cd site in the Cd-Hg alloys. However the ratio of isotropic Knight Shift of 199Hg to 113Cd is somewhat greater than the ratio of 199Hg to 113Cd atomic hyperfine fields suggesting that there is more local electronic "s" character at the Fermi surface in the alloy than in the pure metals. This is consistent with the theoretical picture of Cd in which phonon scattering induced by increasing temperature or alloying smears and weakens the lattice potential which in turn leads to a more "s" like Fermi surface. Further, the 113Cd Knight shift is found to be a useful tool for monitoring the phase segregation that occurs in Cd-Mg due to internal oxidation and for determining the concentrations of solutes such as Hg and Mg in Cd-Hg and Cd-Mg alloys.