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In-situ structural studies of the underpotential deposition of copper onto an iodine-covered platinum surface using x-ray standing waves

We present initial results of an in situ structural investigation of the underpotential deposition of copper on an iodine covered platinum/carbon layered synthetic microstructure, using x-ray standing waves generated by specular (total external) reflection and Bragg diffraction. We also compare the result of surface coverage isotherms derived from both electrochemical and x-ray measurements.