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Hydrogen effects on low cycle fatigue of high strength steels

Abstract Hydrogen absorption occurs during steelmaking processes and causes detriment on mechanical properties, such as plasticity, fatigue strength and tensile strength, among others. The main purpose of the present paper is to study the hydrogen effects on the low cycle fatigue behaviour of a high strength steel, resulphurised and microalloyed. Before the cyclic tests, samples are cathodically charged using a H2SO4 acid solution. In some samples, poisons are added. The flow stress evolution during cycling was studied by analysing the so called ‘back’ and ‘friction’ stresses derived from the hysteresis loops. Fatigued specimens were observed through scanning electron microscopy and transmission electron microscopy. Additionally, the metallographic technique known as ‘silver decoration’ allows evaluation of the hydrogen distribution in the structure by applying energy dispersive analysis. The higher stress levels and cyclic softening rates exhibited by hydrogen charged samples in comparison with uncharged ones are related with the friction stress behaviour. The hydrogen is found mainly associated with MnS inclusions.