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Isothermal curing of an uncatalyzed dicyanate ester monomer : kinetics and modeling

The isothermal cure of a dicyanate ester monomer has been studied under different atmospheres (air and argon) without any catalyst, by following the evolutions of both T g and conversion. Independently of both atmosphere and temperature of cure, there is a unique one-to-one relationship between these two parameters, correctly described by a restated DiBenedetto's equation. The chemical kinetics are satisfactorily modeled with two competing reactions schemes, which are second-order and second-order autocatalyzed, the latter displaying more relative importance under air-curing conditions