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Effect of Phase Transitions on the TSEC and TSEE from Solid Methanol

Thermally Stimulated Electric Current (TSEC) and Thermally Stimulated Exoemission (TSEE) from solid methanol have been measured during a cooling process in the temperature range 170–80 K. Both TSEC and TSEE result from the subjugation of solid methanol to a temperature ramp. It has been found that both TSEC and TSEE intensities depend strongly on whether or not a methanol sample has been cooled diretly from the liquid phase. It has also been found that the TSEC intensity increases with the temperature difference which exists across a sample during the solidification process, whereas the TSEE peak value remains approximately constant for the same conditions. Also, a non-stable broadening of peaks could be observed.