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FLOW SYSTEM FOR ANALYTICAL CALIBRATION BY THE INTEGRATED METHOD

ABSTRACT The flow system has been designed for the purpose of performing analytical determinations according to the integrated calibration method. The system is equipped with a fully rotary valve which serves in preparation of the set of standard solutions from a single stock solution. A standard is exposed to measurements in two forms: by itself, and as a mixture with a sample. Each of the two solutions is able to be propelled to the detector at two different flow rates. As a consequence, the measurement information gathered during a single calibration run permits calculation of several estimations of an analytical result, in both the interpolative and extrapolative manner. Since some estimations are independent of each other, the final result is reliable in terms of accuracy, more than if using a conventional calibration approach. Owing to the instrumental simplicity and analytical efficiency, the system is expected to be useful for routine analysis.