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Integration of a micro reactor system to a ICP mass spectrometer

Hyphenated techniques involving ICP-MS are popular in research and application areas. Micro reactors which are widely integrated to molecular mass spectrometric techniques, however, find little application in the field of atomic spectroscopy in general or ICP-MS in specific. In this work, two integration concepts have been proposed for the integration of a micro reactor system to the Agilent 7700x ICP-MS system. Different tests have been performed using an ICP multi-element standard solution. In both concepts, the micro reactor system was successfully coupled to the ICP-MS that elements of the standard solution from the micro reactor system were detected. In addition, the second concept that includes the ALS enabled standard operations of ICP-MS at start up with warming, calibration and tuning. Finally, a library module of AutoIt software was employed in the control software to automate the operation of the ICP-MS instrument control software.