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Carbothermal Reduction Synthesis of Superfined TiC Powders from TiOSO4

Superfined TiC was successfully synthesized from mixtures of acetylene carbon black and TiSO4 through liquid-phase and subsequent heat treatment at a temperature that was considerably lower than that used in conventional carbonthermal reduction synthesis of TiC. Thermal decomposition of TiSO4, and carbothermal reduction of the mixtures were investigated by using thermogravimetry-differential thermal analyzer and x-ray diffraction analyzer.