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Microwave-Enhanced Coupling of Carboxylic Acids with Liquid Ketones and Cyclic Ethers using TBAI/TBHP.

The oxidative coupling of carboxylic acids with liquid ketones and cyclic ethers has been accomplished in minutes using t-butyl hydroperoxide in the presence of TBAI under microwave irradiation in the absence of a solvent. In addition to drastically shortening the reaction times, the use of microwaves resulted, in general, in yields equal to or higher than those obtained by conventional heating.