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Facile Hydrothermal Synthesis of CoSO4ċH2O Nanoparticles and Barite Microcubes from Novel Precursors

Abstract CoSO4ċH2O nanoparticles and barite (BaSO4) microcubes have been prepared by hydrothermal decomposition of new precursors [Co(tsc)2]Cl2 and [Ba(tsc)2]Cl2 (tsc =  thiosemicarbazide), respectively. The products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and Fourier transform infrared (FT-IR) spectroscopy. As a comparison between two methods, thermal decomposition of novel precursors in high temperature boiling organic solvents were examined.