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Synthesis of NaxMoO3 crystals through high pressure solid-state reaction

ABSTRACT We report growth of high-purity single crystals of the sodium molybdenum bronzes NaxMoO3 through high pressure solid-state reaction routes. Our results demonstrate that the crystallite sizes of NaxMoO3 can rapidly grow to ∼25 μm under a moderate pressure of 4.0 GPa in just 10 min. This discovery provides a starting point for the growth of large single crystals of alkali metal molybdenum bronzes under high pressure.