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Preparation of Porous Carbon Material by Carbonizing Polyacrylonitrile Microspheres

PAN microspheres were crosslinked with divinyl benzene (DVB) and styrene (St), and then pre-oxidized under atmospheric pressure, porous carbon microspheres were produced by carbonizing the pretreated microspheres under nitrogen protection. Morphology and structure characterizations of the materials were performed by employing scanning electron microscopy (SEM), transmission electron microscopy (TEM), nitrogen adsorption test, etc. The results show that the primitive PAN microspheres display flower-like structures, while the carbonized pretreated PAN microspheres exhibit a high porosity as well as specific surface area and have a good adsorption of methylene blue (MeB) dye.