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Pressure Induced Phase Transition in TiB

In situ high pressure x-ray diffraction and electrical resistance experiments on TiB have been carried out by using a diamond anvil cell device. The results revealed that the sample undergoes a first-order phase transition at pressures of 3.5-5.0 GPa and 4.0-5.5 GPa for the x-ray diffraction and electrical resistance experiments, respectively. The parameters of the state equation are calculated before and after the phase transition and compared with the values calculated by Mohn et al. [J. Phys. C: Solid State Phys. 21 (1988) 2829] using the augmented spherical wave method.