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A Neutron Powder Diffraction Investigation of Deuterated Pd15P2*

Crystal structure refinements of pure and deuterated Pd[5P2 have been performed using Rietveld-type profile refinement techniques on neutron powder diffraction intensities. The positions and the degree of occupancy for the dissolved deuterium atoms were determined at 296 K and 500 kPa deuterium pressure. The deuterium atoms were found to occupy distorted tetrahedral interstices between the palladium atoms to an extent corresponding to the formula Pdi5P2Do.46.