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Room‐temperature synthesis and characterization of porous CeO2 thin films

CeO2 thin films with hexagonal‐shaped pores were successfully prepared by a facile electrodeposition at room temperature combined with an etching process. By using electrodeposited ZnO nanorods as a soft template, the morphology, and microstructure of the CeO2 could be controlled. TEM observation indicated that as‐prepared CeO2 film is composed of nanocrystals with average size of several nanometers, while XPS analysis showed the coexistence of Ce3+ and Ce4+ in the film. The photoluminescence properties of CeO2 films were measured, which showed much higher sensitivity compared to bare substrate.