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The Apparent Flexibility of Bonds in Paddlewheel-Type Compounds.

The effect of crystalline environment on the metal−metal and metal−ligand bond lengths is studied in two molecules representative of the compounds containing strong, multiple bonds between two metal atoms and the paddlewheel structural motif. The compounds chosen for this were Ru2(chp)4Cl (chp = 2-chloro-6-oxypyridinate anion) and [Re2Cl8]2-, whose structures were determined from several crystalline forms.