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The Measurement of Wood in Construction Dust Samples: A Furnace Based Thermal Gravimetric Approach.

A furnace-based thermal gravimetric method was developed to measure wood in inhalable construction dust. The application of this method showed that reliance on the inhalable concentrations alone may substantially overestimate carpenters' exposures to wood dust at construction worksites. Test samples were prepared by collecting aerosols of gypsum, calcite, quartz, concrete, and wood dust onto quartz fibre filters using the Button inhalable sampler. The average difference between the measured and loaded mass of wood is 2% over the whole analytical range. Ninety percent of thermogravimetric measurements on all test samples (n = 35) were 13% or less. The limit of detection was measured as 0.065 mg. The thermal gravimetric method was applied to samples collected from four new build construction sites and one shop fitting worksite. The workplace inhalable wood dust results ranged from 15% to 104% of the total inhalable dust values. In addition, an x-ray diffraction (XRD) Rietveld method was applied as a complimentary approach to explain the composition of the remaining inhalable dust. Most combined thermal gravimetric and XRD measurements were within 10% of the total inhalable dust mass values, determined gravimetrically. Ninety-five percent were within 26%. The median proportion of mineral dust containing gypsum, calcite, quartz, dolomite, or rutile was 30%. The proportion of mineral dust on individual filters varied considerably.