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Fine-Tuning of Saponification-Triggered Gelation by Strategic Modification of Peripheral Substituents: Gelation Regulators.

A pioneering approach towards controlling the efficiency of saponification assisted gelation in ethyl ester based ZnII -complexes have been described. Using four new ester containing bis-salen ZnII complexes (C1-C4) involving different para-azo phenyl substituted ligands it has been clearly shown that gelation efficiency is greatly influenced by the electronic effects of the substituents (-H (C1), -CH3 (C2), -NO2 (C3), and -OCH3 (C4)). Morphological, photophysical, and rheological investigations corroborated the experimental observations well and established that gelation efficiency was enhanced with electron-withdrawing characteristics of substituents (C4