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Neutron diffraction and magnetic behavior of ilmenite MnTiO3

A hexagonal symmetry ilmenite MnTiO3 in polycrystalline form with space group R3¯ was prepared by solid state synthesis route. Its phase purity at room temperature was confirmed by X-ray diffraction (XRD) and neutron diffraction (ND) study. The XRD and ND pattern at room temperature could be Rietveld fitted with R3¯ space group. The microscopic parameters are further corroborated by Infra-red spectrum. Temperature dependent magnetization behavior shows additional anomaly at 41K which is not reported earlier. This is associated with two Curie-Weiss temperature θ = 370K and 300K. In addition, our M(H) data confirms the occurrence of anti-ferromagnetic ordering below 100K.