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Crystal structure of GdNi3Ga9

The crystal structure of the GdNi3Ga9 compound was refined on X-ray powder diffraction data collected for a sample of composition Gd7.7Ni23.1Ga69.2. The phase composition determined by X-ray diffraction was confirmed by energy-dispersive X-ray spectroscopy. The refinement of the crystal structure of GdNi3Ga9 was carried using the structure model defined on DyNi3Al9 (Pearson symbol hR99, space group R32, a = 0.72624(1), c = 2.74876(5) nm). The structure type DyNi3Al9 is intermediate between the R0.67Ni2Al6 type in space group P-6m2 (statistical arrangement of rare-earth atoms and Al atom triangles), and the fully ordered structure type ErNi3Al9 with the same supercell and space group R32.