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Interface Reaction between Directional Solidified Superalloy DZ40M and Ceramic Mould

The interfaces between DZ40M directional solidified superalloy and ceramic mould (SiO2-base core and Al2O3-base shell) was studied by scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS). The results showed that there was a serious interface reaction between DZ40M and ceramic cores，which resulted in many reaction pits (~100μm deep), Si rich residue alloys and Zr rich subglobose oxides on the inner surface. And the interface reaction between DZ40M and ceramic shell induced a ~50μm of pink sand burning layer. The thermal analysis showed that the reactions between DZ40M and core or shell were similar: the active alloy constituents (Zr, Al, Ti and Cr) were oxidized and became oxides or solid solution with the core or shell components (SiO2, Al2O3 or Fe2O3), but the interface characterization of DZ40M/core and DZ40M/shell was different because the shell had the main content of Al2O3 and impurity of Fe2O3, while those of the core were SiO2 and CaO, respectively.