N  ~ ~  C  (/J  ~’°  0  \0  ---..)  \0  ---..)  .......  to  N  N  ~  .i;...  TABLE 10  COM- POUND NMR  I-AC  I-AD  I-AE  lH-NMR (400 MHz, DMSO-d6):  I,  (ppm) - 4.61 (dt, 4H, CH2CF2), 3.36  (t, 12H, CH2 inn-butyl), 2.40-2.65 (m,  SH, CH2CH2), 1.72  (s,  6H, CH3), 1.68  (quintet, 12H, CH2 inn-butyl), 1.66 (s,  6H, CH3), 1.35-1.44  (m,  12H, CH2 inn› butyl), 0.81-0.93 (m, 18H, CH3 inn› butyl).  19F-NMR (376 MHz, DMSO-d6):  I,  (ppm)- -111.4.  lH-NMR (400 MHz, DMSO-d6):  I,  (ppm) - 8.29 (d, 8H,ArH), 7.93-8.09  (m, 12H, ArH), 4.61 (dt, 4H, CH2CF2),  2.40-2.65  (m,  SH, CH2CH2), 1.72  (s,  6H, CH3), 1.66  (s,  6H, CH3).  19F-NMR (376 MHz, DMSO-d6):  I,  (ppm)- -47.9, -111.4.  lH-NMR (400 MHz, DMSO-d6):  I,  (ppm) - 7.90-8.24 (m, 14H, ArH),  4.61 (dt, 4H, CH2CF2), 3.85 (s, 6H,  OCH3), 2.42  (s,  12H, ArCH3) 2.40-2.65  (m,  SH, CH2CH2), 1.72  (s,  6H, CH3),  1.66  (s,  6H, CH3).  19F-NMR (376 MHz, DMSO-d6):  I,  (ppm)- -48.8, -111.4.  CATION  PRODUCT  \.  \.  ~s~  ~s~  q,  ~N=N~  ,9  ’J--f  tN  tN  ~  0  /0  0\  0  \.  ~s~  CF3  CF3  10  O3SF2C  CF2SO3  10  USD  USD  q,  r+N=N---h  ,9  J----1  6N  6N  ~  0  /0  0\  0  CF3  10  USD  O3SF2C  CF2SO3  U i:’C?;.3  ~  ui:’C?;.3  ~  q,  r+N=N---h  ,9  ui:’C?;.3  ~  I  I  I  )---ltN  tN~  I  I  #  o  #  #  o  ~ 0  0 ----...  #  #  o  0  /  \  0  I  I  ~~c  ~~  I 