N  .i;...  Ul  C  (/J  ~’°  0  \0  ---..)  \0  ---..)  .......  to  N  N  .i;...  O’I  TABLE  15  COM- POUND NMR  CATION  PRODUCT  I-AR  lH-NMR (400 MHz,  ~  ~  CH;  CH;  ~  DMSO-d6):  I,  (ppm) - 7.75 (s, 4H, Ar), 4.61  ytN-N~O  (dt, 4H, CH2CF2), 3.91- 3.96 (m, 4H, CH2 in  CN  CN  tetramethylenesulfide ),  0  /0  0\  0  3.72-3.79 (m, 4H, CH2  in  O  O  03SF2C  CF2S03  tetramethylenesulfide ),  V  V  V  2.40-2.65 (m,  SH,  CH2CH2), 2.29-2.39  (m,  SH,  CH2 in  tetramethylenesulfide ),  1.75-2.19 (m, 42H,  ArCH3 +Adamantane),  1. 72 (s,  6H,  CH3), 1.66  6  6  6  (s, 6H, CH3).  19F-NMR (376 MHz,  DMSO-d6):  I,  (ppm) - -111.4.  I-AS  lH-NMR (400 MHz,  ~  ~  CH;  CH;  ~  DMSO-d6):  I,  (ppm) - 7.82 (m, 4H,ArH), 4.61  OytN-N~O  (dt, 4H, CH2CF2), 3.73- 3.91 (m, SH CH2 in  CN  CN  pentamethylenesulfide ),  0  /0  0\  0  2.41-2.65 (m, SH,  CH2CH2), 1.56-2.40  O  O  03SF2C  CF2S03  (m,66H,CH3 +  V  V  V  ArCH3 + CH2 in  pentamethylenesulfide +  Adamantane).  19F-NMR (376 MHz,  DMSO-d6):  I,  (ppm) - -111.4.  cs  cs  cs 